A kind of cdte battery back electrode and cdte battery
A back electrode and battery technology, applied in the field of solar cells, can solve the problems of reducing the performance and stability of the battery, easy diffusion, and difficult to control the uniformity of the film layer, so as to achieve good electrical performance, good long-term stability, and improve battery performance. Effect
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[0046] The present invention also provides a kind of preparation method of CdTe battery, comprises the following steps:
[0047] 1) Mixing the C / Cu composite material and the back electrode buffer material, and then placing it to obtain a mixed slurry;
[0048] After treating the CdTe surface of the battery semi-finished product compounded with the CdTe film, a battery semi-finished product with a Te-rich layer on the surface is obtained;
[0049] 2) compounding the mixed slurry on the Te-rich layer of the battery semi-finished product to obtain a battery semi-finished product with a mixed slurry layer compounded on the surface;
[0050] 3) After post-processing the mixed slurry layer, a CdTe battery is obtained.
[0051] In the present invention, the selection and ratio of raw materials in the preparation process of the CdTe battery and other optimization principles, unless otherwise specified, correspond to the uniformity of the aforementioned CdTe battery and the back elec...
Embodiment 1
[0063] Firstly, prepare C / Cu raw materials. Since C / Cu nanomaterials have agglomeration, they should be ground and filtered before use to make them disperse faster and more uniformly in the slurry. C / Cu nanomaterials (Zunye Nanomaterials Co., Ltd.) were ground in an agate mortar until there were no agglomerated particles, and the ground C / Cu was filtered through a 400-mesh sieve.
[0064] Carry out TEM test to the C / Cu nanocomposite material that above-mentioned steps obtains, see figure 2 , figure 2 Transmission electron microscope image of the C / Cu composite material prepared for the present invention. Depend on figure 2 It can be seen that the particle size of the C / Cu composite material is about 100nm. In the lower right corner of the figure, it can be seen that more black substances are agglomerated together, and the color of the edge part is lighter. The particle size in the middle of the picture is about 50nm, and it can be clearly seen that the darker part of the...
Embodiment 2
[0099] In the production process, when the slurry configuration and aging time are insufficient, the battery efficiency can be improved by annealing after the battery is completed.
[0100] As in the slurry configuration of Example 1, prepare a slurry with a suitable viscosity of 0.5% C / Cu content, and the stirring and standing time is shortened to half of that of Example 1.
[0101] Using TCO film as substrate, using rf magnetron sputtering process, in 10mTorr vacuum, O 2 / Ar about 2% atmosphere, 200W power, deposit a layer of polycrystalline CdS film on it, about 100nm. Transfer the sample to a close-range sublimation device with a source temperature of 660°C, a substrate temperature of 560°C, and a vacuum of 8 Torr, O 2 / N 2 In an atmosphere with a content of about 1.5%, polycrystalline CdTe of 5-6 μm is deposited on the CdS film layer to obtain a battery semi-finished product compounded with a CdTe film.
[0102] Then the CdTe surface was treated with NP solution. NP s...
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