Preparation method for graphene-modified visible abrasion-resistant coating
A graphene modification and wear-resistant coating technology, applied in the coating, metal material coating process, melt spraying and other directions, can solve the problem that the test process is not intuitive, the bonding strength of the coating layer is low, and the coating is easy to age and fail. and other problems to achieve the effect of monitoring the integrity of the coating and the safe service status
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Embodiment 1
[0035] On the basis of the foregoing embodiments, a method for preparing a graphene-modified visible wear-resistant coating provided in this embodiment comprises the following steps:
[0036] Step (1) Weigh 20g of strontium carbonate (SrCO 3 ), 10g of alumina (Al 2 o 3 ), weigh 300ml of alcohol, and place the mixed powder and alcohol in a planetary ball mill for ball milling and mixing for 60 minutes until the alcohol is completely volatilized. Then it was transferred to a corundum boat and treated in a high-temperature furnace at a temperature of 900 °C for 4 h.
[0037] Step (2) Weigh 1 g of graphene oxide and disperse it in 100 ml of absolute ethanol with ultrasonic vibration to prepare a graphene oxide dispersion. The ultrasonic dispersion time is 120min, and the ultrasonic frequency is 15Hz.
[0038] Step (3) weigh 2g europium oxide (Eu 2 o 3 ) and 2g dysprosium oxide (Dy 2 o 3 ), add 300ml of dilute hydrochloric acid to dissolve, and add 300ml of distilled water ...
Embodiment 2
[0047] On the basis of the foregoing embodiments, a method for preparing a graphene-modified visible wear-resistant coating provided in this embodiment comprises the following steps:
[0048] Step (1) Weigh 30g of strontium carbonate (SrCO 3 ), 15g of alumina (Al 2 o 3 ), weigh 500ml of alcohol, and place the mixed powder and alcohol in a planetary ball mill for ball milling and mixing for 70 minutes until the alcohol is completely volatilized. Then it was transferred to a corundum boat and treated in a high-temperature furnace at a temperature of 1000 °C for 5 h.
[0049] Step (2) Weigh 2 g of graphene oxide and disperse it in 200 ml of absolute ethanol with ultrasonic vibration to prepare a graphene oxide dispersion. The ultrasonic dispersion time is 120min, and the ultrasonic frequency is 15Hz.
[0050] Step (3) weigh 3g europium oxide (Eu 2 o 3 ) and 1.5g dysprosium oxide (Dy 2 o 3 ), add 500ml of dilute hydrochloric acid to dissolve, and add 500ml of distilled wat...
Embodiment 3
[0056] On the basis of the foregoing embodiments, a method for preparing a graphene-modified visible wear-resistant coating provided in this embodiment comprises the following steps:
[0057] Step (1) Weigh 60g of strontium carbonate (SrCO 3 ), 40g of alumina (Al 2 o 3 ), weigh 600ml of alcohol, and place the mixed powder and alcohol in a planetary ball mill for ball milling and mixing for 80 minutes until the alcohol is completely volatilized. Then it was transferred to a corundum boat and treated in a high-temperature furnace at a temperature of 1000 °C for 6 h.
[0058] Step (2) Weigh 1 g of graphene oxide and disperse it in 100 ml of absolute ethanol with ultrasonic vibration to prepare a graphene oxide dispersion. The ultrasonic dispersion time is 120min, and the ultrasonic frequency is 15Hz.
[0059] Step (3) weigh 3g europium oxide (Eu 2 o 3 ) and 2g dysprosium oxide (Dy 2 o 3 ), add 300ml of dilute hydrochloric acid to dissolve, and add 300ml of distilled water...
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