A kind of hollow porous nano-α-fe 2 o 3 Preparation and Application of Hexagonal Prism Materials
A hexagonal prism, hollow porous technology, applied in the field of energy materials and electrochemistry, can solve the problems of hexagonal prism materials that have not been reported, and achieve good comprehensive electrochemical performance, conducive to transmission, and controllable process parameters.
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Embodiment 1
[0031]Stir 0.2 g of fumaric acid, 1 g of ferric nitrate nonahydrate and 60 mL of DMF at room temperature for 1 h to obtain a clear mixture. The mixed solution was transferred to an oil bath to react for 40 minutes, the product was centrifuged, washed with DMF and anhydrous methanol three times successively, and the obtained product was dried in a vacuum oven to obtain Fe-MIL-88A. Put 0.25g Fe-MIL-88A, 50mL water, 50mL absolute ethanol, and 0.2g sodium hydroxide in a beaker and stir for 5h. The resulting product was washed with absolute ethanol and dried in vacuum at 50°C to obtain nanohollow porous nano-α-Fe 2 o 3 Hexagonal prism material powder.
[0032] The prepared 50wt.% nano-hollow porous nano-α-Fe 2 o 3 Hexagonal prism material, 30wt.% acetylene black and 20wt.% PVDF are mixed evenly to make a slurry, evenly coated on copper foil, vacuum dried and punched into circular electrode pole pieces, with metal lithium as the counter electrode Make up the test battery. The ...
Embodiment 2
[0034] 0.4 g of fumaric acid, 1.6 g of ferric nitrate nonahydrate and 40 mL of DMF were stirred at room temperature for 40 min to obtain a clear mixture. The mixed solution was transferred to an oil bath to react for 1.5 h, the product was centrifuged, washed with DMF and anhydrous methanol three times successively, and the obtained product was dried in a vacuum oven to obtain Fe-MIL-88A. Put 0.4g Fe-MIL-88A, 100mL absolute ethanol, and 1.2g sodium hydroxide in a beaker and stir for 3h. The resulting product was washed with absolute ethanol and dried in vacuum at 50°C to obtain nanohollow porous nano-α-Fe 2 o 3 Hexagonal prism material powder.
[0035] The prepared 50wt.% nano-hollow porous nano-α-Fe 2 o 3 Hexagonal prism material, 30wt.% acetylene black and 20wt.% PVDF are mixed evenly to make a slurry, evenly coated on copper foil, vacuum dried and punched into circular electrode pole pieces, with metal lithium as the counter electrode Make up the test battery. Figure...
Embodiment 3
[0037] 1 g of fumaric acid, 3.5 g of ferric nitrate nonahydrate and 230 mL of DMF were stirred at room temperature for 1 h to obtain a clear mixture. The mixed solution was transferred to an oil bath to react for 40 minutes, the product was centrifuged, washed with DMF and anhydrous methanol three times successively, and the obtained product was dried in a vacuum oven to obtain Fe-MIL-88A. Put 1g of Fe-MIL-88A, 200mL of water, 400mL of absolute ethanol, and 3g of sodium hydroxide in a beaker and stir for 7h. The resulting product was washed with absolute ethanol and dried in vacuum at 50°C to obtain nanohollow porous nano-α-Fe 2 o 3 Hexagonal prism material powder.
[0038] The prepared 50wt.% nano-hollow porous nano-α-Fe 2 o 3 Hexagonal prism material, 30wt.% acetylene black and 20wt.% PVDF are mixed evenly to make a slurry, evenly coated on copper foil, vacuum dried and punched into circular electrode pole pieces, with metal lithium as the counter electrode Make up the ...
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