Salix matsudana branch cortex chloroplast preparation method
A chloroplast and switchgear technology, applied in the field of agricultural biology, can solve the problems such as no preparation method, public report and the like of chloroplast in the bark of Salix chinensis.
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Embodiment 1
[0021] Embodiment 1 prepares willow branch cortex chloroplast with the method of the present invention
[0022] 1) Sampling and homogenization: in the early morning of the growing season, take the bark of the current year's branches of willow, wash it with deionized water, dry it with filter paper, and cut the bark into 5mm 2 Take 20g of bark pieces and transfer them to a homogenizer (WARING, USA), add 200mL of separation liquid (Table 1), and homogenize twice at slow speed and fast speed, each time for 5 seconds, with an interval of 1 minute.
[0023] 2) Filtration: filter the homogenate through 4 layers of gauze, and collect the filtrate in an ice-bathed beaker.
[0024] 3) Preparation of coarse chloroplast precipitate: Divide the filtrate evenly into 50 mL centrifuge tubes, centrifuge at 200 g for 3 min in an angle rotor, transfer the supernatant to a new centrifuge tube, and centrifuge at 1500 g for 10 min to obtain coarse chloroplast precipitate.
[0025] 4) Suspension o...
Embodiment 2
[0031] Example 2 Chloroplast Fluorescence Microscopic Examination
[0032] The chloroplast suspension obtained in the present invention was dropped on the center of the glass slide, covered with a cover glass to prepare a temporary mount, and examined with a fluorescence microscope (Imager.A1, Zeiss). Observe the images of chloroplasts in bright field to judge whether there is contamination of other organelles in the field of view; observe the images of chlorophyll fluorescence of chloroplasts under excitation light to judge the activity of chloroplasts. The results showed that the chloroplasts were scattered and distributed in the bright field, and no contamination of other cell components was found; under the excitation light, the chloroplasts all had chlorophyll fluorescence, and the chloroplasts had photosynthetic activity.
Embodiment 3
[0033] Embodiment 3 Chloroplast capsule integrity inspection
[0034] The potassium ferricyanide method is used to test the capsule integrity of the chloroplast obtained in the present invention. Take two equal-volume chloroplast suspensions, one of which is burst in deionized water, and the other is not subjected to bursting treatment, and the oxygen release rate of the two chloroplasts is detected with an oxygen electrode (Chlorolab2, Hansatech) respectively, and calculated according to formula 1 The integrity rate of the chloroplast capsule, it can be determined that the integrity rate of the chloroplast prepared by the method of the present invention is 87%.
[0035] Formula 1:
PUM
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