Preparation method of composite algicide
An algaecide and the technology of preparation steps are applied in the field of compound algaecide preparation, which can solve the problems of low long-term algae killing rate, high local chemical concentration, and short effective time of chemical algae killing, so as to increase the specific surface area, Strong adsorption and the effect of improving the efficiency of algae removal
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example 1
[0026]Weigh the montmorillonite and soak it in hydrochloric acid with a concentration of 0.5mol / L for 1 hour, take it out, spray and freeze it with liquid nitrogen immediately for 2 minutes, and then put the frozen montmorillonite in an oven at 105°C for 1 hour to obtain pretreated montmorillonite soil; according to the mass ratio of 1:3, the mass fraction is 30% cobalt nitrate solution and the mass fraction is 20% ferric nitrate solution to mix to obtain a mixed solution, and the above pretreatment montmorillonite is soaked in 1mol / L citric acid solution for 20min After taking it out, immediately pour it into the mixed solution and continue soaking for 30 minutes to obtain the reaction mixed solution; adjust the pH of the above reaction mixed solution to 7.3 with 20% ammonia water by mass fraction, and heat up to 60°C, stir and mix for 20 minutes, filter, and separate to obtain the filter residue , transfer the obtained filter residue into a muffle furnace, heat-preserve and c...
example 2
[0028] Weigh the montmorillonite and soak it in 0.5mol / L hydrochloric acid for 1 hour, take it out, spray and freeze it with liquid nitrogen immediately for 2 minutes, then put the frozen montmorillonite in an oven and dry it at 108°C for 2 hours to obtain pretreated montmorillonite soil; according to the mass ratio of 1:3, the mass fraction is 30% cobalt nitrate solution and the mass fraction is 20% ferric nitrate solution to mix to obtain a mixed solution, and the above-mentioned pretreatment montmorillonite is soaked in 1mol / L citric acid solution for 25min After taking it out, immediately pour it into the mixed solution and continue soaking for 35 minutes to obtain the reaction mixed solution; adjust the pH of the above reaction mixed solution to 7.4 with 20% ammonia water by mass fraction, and heat up to 65°C, stir and mix for 25 minutes, filter, and separate to obtain the filter residue , transfer the obtained filter residue into a muffle furnace, heat-preserve and calcin...
example 3
[0030] Weigh the montmorillonite and soak it in hydrochloric acid with a concentration of 0.5mol / L for 2 hours, take it out, immediately spray and freeze it with liquid nitrogen for 3 minutes, then put the frozen montmorillonite in an oven and dry it at 110°C for 2 hours to obtain pretreated montmorillonite Soil; be 1:3 by mass fraction be that 30% cobalt nitrate solution and mass fraction are 20% ferric nitrate solution to mix to obtain mixed solution, above-mentioned pretreatment montmorillonite concentration is that 1mol / L citric acid solution soaks 30min After taking it out, immediately pour it into the mixed solution and continue soaking for 40 minutes to obtain the reaction mixed solution; adjust the pH of the above reaction mixed solution to 7.5 with 20% ammonia water by mass fraction, and heat up to 70°C, stir and mix for 30 minutes, filter, and separate to obtain the filter residue , transfer the obtained filter residue into a muffle furnace, heat-preserve and calcinat...
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