Fabric dyeing deepening agent and preparation method thereof
A fabric dyeing and darkening agent technology, which is applied in textiles, papermaking, fiber treatment, etc., can solve the problems of poor color fastness of fabrics and poor darkening effect of fabric darkening agents, so as to improve interface compatibility and avoid Decreases sharply, increases the effect of the deepening effect
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example 1
[0024] In parts by weight, take 20 parts of urethane acrylate, 10 parts of perfluoroundecyl acrylate, 10 parts of trifluoroethyl methacrylate, 10 parts of tetrahydrofuran acrylate, and pour them into the mixing machine at 300r Stir and mix for 45 minutes at a speed of 1 / min, and discharge the material to obtain an organic resin. Then, in parts by weight, take 30 parts of ethyl orthosilicate and 80 parts of a 60% ethanol solution by mass. First, pour the ethanol solution into a three-necked flask. Move the three-necked flask into a digital speed-measuring thermostatic magnetic stirrer, and adjust the pH of the ethanol solution to 2.0 with a mass fraction of 6-8% hydrochloric acid at a temperature of 45°C and a rotational speed of 300r / min. After the pH adjustment is over, Under constant temperature stirring, add ethyl orthosilicate to the three-necked flask through a dropping funnel at a rate of 3mL / min. After the addition of ethyl orthosilicate is finished, continue constant tem...
example 2
[0026] In parts by weight, take 20 parts of urethane acrylate, 10 parts of perfluoroundecyl acrylate, 10 parts of trifluoroethyl methacrylate, 10 parts of tetrahydrofuran acrylate, and pour them into the mixing machine at 300r Stir and mix for 45 minutes at a speed of 1 / min, and discharge the material to obtain an organic resin. Then, in parts by weight, take 30 parts of ethyl orthosilicate and 80 parts of a 60% ethanol solution by mass. First, pour the ethanol solution into a three-necked flask. Move the three-necked flask into a digital speed-measuring constant-temperature magnetic stirrer, and adjust the pH of the ethanol solution to 2.0 with a mass fraction of 6-8% hydrochloric acid at a temperature of 45°C and a rotational speed of 300r / min. After the pH adjustment is over, Under constant temperature stirring, add ethyl orthosilicate to the three-necked flask through a dropping funnel at a rate of 3mL / min. After the addition of ethyl orthosilicate is finished, continue cons...
example 3
[0028] In parts by weight, take 20 parts of urethane acrylate, 10 parts of perfluoroundecyl acrylate, 10 parts of trifluoroethyl methacrylate, 10 parts of tetrahydrofuran acrylate, and pour them into the mixing machine at 300r Stir and mix for 45 minutes at a speed of 1 / min, and discharge the material to obtain an organic resin. Then, in parts by weight, take 30 parts of ethyl orthosilicate and 80 parts of a 60% ethanol solution by mass. First, pour the ethanol solution into a three-necked flask. Move the three-necked flask into a digital speed-measuring constant-temperature magnetic stirrer, and adjust the pH of the ethanol solution to 2.0 with a mass fraction of 6-8% hydrochloric acid at a temperature of 45°C and a rotational speed of 300r / min. After the pH adjustment is over, Under constant temperature stirring, add ethyl orthosilicate to the three-necked flask through a dropping funnel at a rate of 3mL / min. After the addition of ethyl orthosilicate is finished, continue cons...
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