Microsphere suspended seed coating agent and preparation method thereof
A technology of suspended seed coating agent and microspheres, applied in the field of pesticides, can solve the problems of short duration of effect of conventional suspended seed coating agent, low utilization rate of active ingredients, single control effect, etc., and achieve stable drug effect and long duration of effect. , the effect of low cost of control
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[0036] The specific steps of the preparation method of flufenoxam-clothianidin microsphere suspension seed coating agent are as follows:
[0037](1) The preparation method of fenfluxam-clothianidin microspheres: according to the ratio of raw materials, respectively take a certain mass ratio of fenfluxam, clothianidin and polylactic acid, and use dichloromethane Dissolve completely, airtight container and be placed in ice-water bath (weigh in the dissolving process, add methylene chloride in time to replenish the weight of loss), inject the medicinal solution into a certain amount of emulsifier containing 0.05% Tween- In the 80 aqueous solution, emulsify with a high-speed stirrer at 3000-4500rpm for 30-40S to obtain the primary emulsion (add 0.1-0.3ml of silicone defoamer depending on the amount of foam in the primary emulsion), and quickly pour the resulting solution into a dispersing and stirring device In a beaker, keep the reaction temperature at 30-35°C, stir at 500-800rpm...
Embodiment 1
[0040] Example 1 (Sample 1): 2.5% Cycloxam-clothianidin Microsphere Suspension Seed Coating Agent (Fluorine:Thiazide=1:6)
[0041] Raw material formula: 13.75 grams of 18.22% fenfluxam-clothianidin microspheres (fluoro:thiazide = 1:6), 1.24 grams of dispersant SP-2836, 0.88 grams of sodium lauryl sulfate, 0.81 grams of magnesium aluminum silicate , xanthan gum 0.11 g, urea 3.11 g, silicone defoamer 0.22 g, preservative S-300.18 g, film-forming agent Km-M0 11.85 g, colorant Red-8110 3.12 g, water to 100 g.
Embodiment 2
[0042] Example 2 (sample 2): 10% fenfluxam-clothianidin microsphere suspension seed coating (fluorine: thiothiazine = 1:6)
[0043] Raw material formula: 18.22% fenfluxam-clothianidin microspheres (fluoro:thiazide = 1:6) 54.77 grams, polyoxyethylene polyoxypropylene block copolymer Atlox 49131.54 grams, NN-89060.61 grams, xanthan gum 0.06 grams, 3.02 grams of ethylene glycol, 0.22 grams of silicone defoamer, 0.22 grams of preservative S-300, 3.02 grams of film-forming agent Km-M01, 6.04 grams of coloring agent Red-8110, water to 100 grams.
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