Method for preparing foam metal through resin microsphere stacking
A technology of foamed metal and resin microspheres is applied in the field of foamed metal preparation, which can solve the problems of complicated operation, slow deposition speed, difficult to master, etc., and achieves the effect of simplifying the technological process, simple and easy operation, and not easy to plastic deformation.
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[0029] Example 1
[0030] A method for preparing foamed metal by stacking resin microspheres. The specific process for preparing foamed metal copper is as follows:
[0031] Make 10kg ethanol and 10kg water into a mixed solvent, then dissolve 2kg methyl methacrylate monomer, 0.3kg polyvinylpyrrolidone, 0.03kg azobisisobutyronitrile in the mixed solvent, add a stirrer, reflux condenser and In the reactor of the aeration system, air is blown in while stirring, so that the gas generates uniform and stable bubbles in the reaction system, and the temperature is raised to 70°C for polymerization reaction. After completion of the reaction for 5 hours, it was separated by centrifugal sedimentation, washed several times with absolute ethanol, and dried under vacuum at 55°C for 22 hours to obtain hollow PMMA microspheres; take the foaming mold, transport the PMMA microspheres into the foaming mold through airflow, and Keep the airflow impacted for 3 minutes, then stop the air flow, and let t...
Example Embodiment
[0034] Example 2
[0035] A method for preparing foamed metal by stacking resin microspheres. The specific process for preparing foamed metal copper is as follows:
[0036] Make 10kg ethanol and 10kg water into a mixed solvent, then dissolve 2kg methyl methacrylate monomer, 0.3kg polyvinylpyrrolidone, 0.03kg azobisisobutyronitrile in the mixed solvent, add a stirrer, reflux condenser and In the reactor of the aeration system, air is introduced while stirring, so that the gas generates uniform and stable bubbles in the reaction system, and the temperature is raised to 70°C for polymerization. After completion of the reaction for 5 hours, it was separated by centrifugal sedimentation, washed several times with absolute ethanol, and dried under vacuum at 55°C for 22 hours to obtain hollow PMMA microspheres; take the foaming mold, transport the PMMA microspheres into the foaming mold through airflow, and Keep the airflow impacted for 2 minutes, then stop the air flow, and let the mold...
Example Embodiment
[0039] Example 3
[0040] A method for preparing foamed metal by stacking resin microspheres. The specific process for preparing foamed metal copper is as follows:
[0041] Make 10kg ethanol and 10kg water into a mixed solvent, then dissolve 2kg methyl methacrylate monomer, 0.3kg polyvinylpyrrolidone, 0.03kg azobisisobutyronitrile in the mixed solvent, add a stirrer, reflux condenser and In the reactor of the aeration system, air is introduced while stirring, so that the gas generates uniform and stable bubbles in the reaction system, and the temperature is raised to 70°C for polymerization. After completion of the reaction for 5 hours, centrifugal sedimentation and separation, and washing with absolute ethanol several times, vacuum drying at 55 ℃ for 22 hours to obtain hollow PMMA microspheres; take the foaming mold, transport the PMMA microspheres into the foaming mold through airflow, and Keep the airflow impact for 3 minutes, then stop the air flow, and let the mold stand for ...
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