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Preparation method of pattered metallic textile on the basis of pretreatment with dopamine

A patterned metal and dopamine technology, applied in textiles and papermaking, fiber treatment, metal material coating technology, etc., can solve the problems of unfriendly environment, complex process, lower sintering temperature, etc., and achieve good conductivity and electromagnetic shielding performance , uniform coating and simple process

Inactive Publication Date: 2018-03-02
DONGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

(1) Metal fibers are mixed into textiles by weaving, but the process is more complicated and the design pattern is limited, because the conductive pattern needs to follow the warp and weft directions in the fabric
(2) Use the printing method to print ink or paste containing metal nanoparticles on the surface of the fabric. This method has complete design freedom and can produce a variety of conductive metal patterns, but because this method requires high temperature in the later stage Sintering volatilizes excess stabilizers and organic solvents to achieve the best conductive effect of metal nanoparticles, which has a certain risk of thermal degradation and thermal deformation for textile substrates, and lowering the sintering temperature will cause the remaining of stabilizers. The electrical conductivity is reduced. In addition, high temperature sintering will easily cause damage to the surface of the fabric. The bonding degree between the metal layer and the surface of the fabric is not high enough, which is not friendly to the environment.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Preparation method of pattered metallic textile on the basis of pretreatment with dopamine
  • Preparation method of pattered metallic textile on the basis of pretreatment with dopamine
  • Preparation method of pattered metallic textile on the basis of pretreatment with dopamine

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] (1) Adjust the pH value of the dopamine solution with a concentration of 2 mg / mL to 8.5 with tris-hydrochloric acid buffer solution, then gently stir at 25°C for 24 hours to oxidize and self-polymerize to form polydopamine, and add alginic acid Sodium adjusts the viscosity to 5000-10000cP to form a dopamine-modified slurry.

[0042] (2) Print the dopamine-modified slurry obtained in step (1) on the surface of the polyester fabric to form a pattern by screen printing technology, dry at 60°C for 20 minutes, and then repeat printing and drying to obtain a dopamine-modified pattern Polyester base.

[0043] (3) Immerse the dopamine-modified patterned polyester substrate obtained in step (2) in 1% AgNO 3 After 24 hours in the solution, it was taken out, washed with distilled water, and dried at 60° C. for 20 minutes to obtain an activated patterned polyester substrate.

[0044] (4) To 40g / L AgNO 3Add ammonia water dropwise to the solution from cloudy to clear, then add 120...

Embodiment 2

[0047] (1) Adjust the pH value of the dopamine solution with a concentration of 2 mg / mL to 8.5 with tris-hydrochloric acid buffer solution, then gently stir at 25°C for 24 hours to oxidize and self-polymerize to form polydopamine, and add alginic acid Sodium adjusts the viscosity to 5000-10000cP to form a dopamine-modified slurry.

[0048] (2) Print the dopamine-modified slurry obtained in step (1) on the surface of the polyester fabric to form different patterns by screen printing technology, dry at 60°C for 20 minutes, and then repeat printing and drying to obtain dopamine-modified Patterned polyester base.

[0049] (3) Immerse the dopamine-modified patterned polyester substrate obtained in step (2) in 1% AgNO 3 and polyvinylpyrrolidone in a mixed solution for 24 hours, then taken out, washed with distilled water, and dried at 60°C for 20 minutes to obtain an activated patterned polyester substrate.

[0050] (4) To 40g / L AgNO 3 Add ammonia water dropwise to the solution f...

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Abstract

The invention relates to a preparation method of a pattered metallic textile on the basis of pretreatment with dopamine. The preparation method includes the steps of: 1) performing oxidizing auto-polymerization to a dopamine solution to obtain polydopamine, and adding slurry to obtain dopamine-modified slurry; 2) printing the surface of a Dacron fabric through a printing technology to form a pattern, drying the fabric, repeatedly printing the fabric, drying the fabric to obtain a dopamine-modified pattered polyester substrate; 3) impregnating the pattered polyester substrate in an activating solution, and washing and drying the substrate to obtain activated pattered polyester substrate; 4) placing the activated pattered polyester substrate in a metal plating solution to perform chemical-plating in a deposition manner, and cleaning and drying the product to obtain the pattered metallic textile on the basis of pretreatment with dopamine. Through the chemical-plating method, the conductive fabric is produced. Compared with other surface treatment technologies, the preparation method is free of external power supply and has simple operation and simple processes. The plated layer is relatively uniform. The method also allows deposition on non-metallic fabrics, and the produced textile has high electric-conductivity and good electromagnetic shielding performance, is low in cost and is more economical and environment-friendly.

Description

technical field [0001] The invention belongs to the technical field of flexible electronics, in particular to a method for preparing patterned metal textiles based on dopamine pretreatment. Background technique [0002] Wearable flexible electronics has gradually developed into a key research project because of its advantages that traditional electronics cannot achieve, such as lightness, bendability, flexibility, etc., and it has also been used in many fields, such as smart sportswear , patient vital sign monitoring, portable sensors, fabric-based electronic entertainment devices, and military electronically functional uniforms, among others. Therefore, the effective combination of textiles and electronics can further expand the application field of textiles. [0003] Polyester is a synthetic fiber with the fastest development, the highest output and the widest range of applications. It has good performance and low price. It has been widely used in many aspects of national...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M11/83D06M15/37D06M15/11D06M15/13D06M15/03D06M15/263C23C18/16C23C18/30C23C18/31D06M101/32
CPCD06M11/83C23C18/1608C23C18/30C23C18/31D06M15/03D06M15/11D06M15/13D06M15/263D06M15/37D06M2101/32
Inventor 俞丹茅昀王炜
Owner DONGHUA UNIV
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