Method for preparing antimony-doped tin oxide electrochromic film
An antimony-doped tin oxide and electrochromic technology, applied in the field of optoelectronics, can solve the problems of not being suitable for mass production, high loss rate of TCO nanoparticles, and long material preparation time, so as to achieve high film preparation efficiency and short coating time , the effect of controllable grain size
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[0017] The present invention provides a method for preparing antimony-doped tin oxide electrochromic film. The specific steps are as follows:
[0018] Step 1. Prepare spraying solution: first add antimony trichloride to acetylacetone, stir at 50℃~60℃ for 30min, then add tin tetrachloride pentahydrate, continue stirring at 50℃~60℃ for 1 hour, wait After the mixed solution is cooled to room temperature, add acetic anhydride and stir at room temperature for 30 minutes, and finally add absolute ethanol, and stir at room temperature for 20 minutes to obtain an ATO spray solution;
[0019] In step 1, the raw material ratio of the ATO spray solution is: the molar ratio of tin tetrachloride, antimony chloride, absolute ethanol, acetylacetone and acetic anhydride is 1:0.01~0.05:45~50:4~7.2: 1.0~2.0;
[0020] Step 2. Preparation of ATO film: first put the soda-lime glass substrate into a heating furnace and heat it to 350℃~450℃, and then move it to the spraying room by the transmission device...
Example Embodiment
[0026] Example 1
[0027] A preparation method of antimony-doped tin oxide electrochromic film, the specific steps are as follows:
[0028] First, prepare spray solution: add 0.65g antimony trichloride to 114.23g acetylacetone, stir magnetically at 50℃ for 30min, then add 100g tin tetrachloride pentahydrate, continue magnetic stirring at 50℃ for 1 hour to obtain orange Yellow solution. After the solution was cooled to room temperature, 29.12g of acetic anhydride was added to it and stirred at room temperature for 30min, and finally 591.23g of absolute ethanol was added and stirred at room temperature for 20min to obtain an ATO spray solution with stable performance. Among them, the spraying liquid ratio is: the molar ratio of tin tetrachloride, antimony chloride, absolute ethanol, acetylacetone and acetic anhydride is 1:0.01:45:4:1.0.
[0029] Then, ultrasonic spray pyrolysis film formation. Clean the ordinary soda-lime glass substrate, put it in a heating furnace and heat it. Whe...
Example Embodiment
[0031] Example 2
[0032] A preparation method of antimony-doped tin oxide electrochromic film, the specific steps are as follows:
[0033] First, prepare spray solution: add 2.60g antimony trichloride to 171.34g acetylacetone, stir magnetically at 55°C for 30min, then add 100g tin tetrachloride pentahydrate, continue magnetic stirring at 55°C for 1 hour to obtain orange Yellow solution. After the solution was cooled to room temperature, 43.68g of acetic anhydride was added and stirred at room temperature for 30min, and finally 617.57g of absolute ethanol was added and stirred at room temperature for 20min to obtain an ATO spray solution with stable performance. Among them, the spraying liquid ratio is: the molar ratio of tin tetrachloride, antimony chloride, absolute ethanol, acetylacetone and acetic anhydride is 1:0.04:47:6:1.5.
[0034] Then, ultrasonic spray pyrolysis film formation. Clean the ordinary soda-lime glass substrate, put it in a heating furnace and heat it. When th...
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