Refractory material with high strength and mechanical property
A refractory, high-strength technology, applied in the field of refractory research and development, can solve the problems of unfavorable recycling, difficult recycling, general mechanical properties, etc. The effect of improved performance
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Embodiment 1
[0018] A refractory material with high strength and mechanical properties, which is made of the following components in terms of mass percentage: 23% zirconia, 18% silica, 2.0% alumina, 1.0% iron oxide, 0.6% titanium dioxide, The rare earth component accounts for 0.3%, and the rest is pyrite slag, and its preparation method comprises the following steps:
[0019] (1) Dry pyrite slag at 100°C to constant weight, then grind it with a ball mill until it passes through an 80-mesh sieve to obtain pyrite slag fine powder, and calcinate the pyrite slag fine powder at 1150°C for 2 hours , to prepare slag clinker;
[0020] (2) Mix zirconia and silica, add sulfuric acid with a concentration of 80% and soak for 30 minutes, remove and rinse until neutral, then calcinate at 680°C for 3 hours, then mix with slag clinker, alumina, iron oxide, Mix titanium dioxide and rare earth components, add water with a mass percentage of 8%, stir evenly and stale for 15 hours;
[0021] (3) Put the stal...
Embodiment 2
[0028] A refractory material with high strength and mechanical properties, which is made of the following components in terms of mass percentage: 24% zirconia, 19% silica, 2.2% alumina, 1.1% iron oxide, 0.7% titanium dioxide, The rare earth component accounts for 0.4%, and the rest is pyrite slag, and its preparation method comprises the following steps:
[0029] (1) Dry pyrite slag at 105°C to constant weight, then grind it with a ball mill until it passes through a 90-mesh sieve to obtain pyrite slag fine powder, and calcinate the pyrite slag fine powder at 1200°C for 2.5 hours , to prepare slag clinker;
[0030] (2) Mix zirconia and silica, add sulfuric acid with a concentration of 90% and soak for 35 minutes, remove and rinse until neutral, then calcinate at 700°C for 3.5 hours, then mix with slag clinker, alumina, iron oxide, Mix titanium dioxide and rare earth components, add water with a mass percentage of 9%, stir evenly and stale for 16 hours;
[0031] (3) Put the s...
Embodiment 3
[0038] A refractory material with high strength and mechanical properties, which is made of the following components in terms of mass percentage: 25% zirconia, 20% silica, 2.5% alumina, 1.2% iron oxide, 0.8% titanium dioxide, The rare earth component accounts for 0.5%, and the rest is pyrite slag, and its preparation method comprises the following steps:
[0039] (1) Dry the pyrite slag at 110°C to constant weight, then grind it with a ball mill until it passes through a 80-100 mesh sieve to obtain fine pyrite slag powder, and calcinate the pyrite slag fine powder at 1250°C 3 hours, prepared slag clinker;
[0040] (2) Mix zirconia and silica, add sulfuric acid with a concentration of 95% and soak for 40 minutes, remove and rinse until neutral, then calcinate at 720°C for 4 hours, then mix with slag clinker, alumina, iron oxide, Mix titanium dioxide and rare earth components, add water with a mass percentage of 10%, stir evenly and stale for 18 hours;
[0041] (3) Put the sta...
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