Preparation method of enhanced polycarboxylate superplasticizer
A technology of polycarboxylate and water reducer, which is applied in the field of preparation of enhanced polycarboxylate water reducer, can solve the problems of large investment in fixed assets, slow production efficiency, long production process, etc., and achieve good economic and social benefits , easy operation, fast response effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0017] (1) Graphene oxide modified polyether monomer: At 70-80°C, allyl polyoxyethylene ether and graphene oxide reacted for 5-8 hours under the catalysis of p-toluenesulfonic acid to obtain a modified polyether monomer. ether monomer. Wherein the mass ratio of allyl polyoxyethylene ether, graphene oxide and p-toluenesulfonic acid is: 100:5:3.
[0018] (2) Add the modified polyether monomer and water prepared in step (1) into the reactor to dissolve, put the reactor under ultraviolet light, and add the first solution and the second solution dropwise at a constant speed within 1-2h Carry out the polymerization reaction, after the dropwise addition, react at a constant temperature for 1 hour, add sodium hydroxide solution to neutralize to pH = 6-7, and obtain the enhanced polycarboxylate water reducer. Wherein the first solution is an aqueous solution of 2-methyl-1-(4-methylthiophenyl)-2-morpholino-1-propanone and 3,6-dioxo-1,8-octanedithiol, The second solution is an aqueous ...
Embodiment 2
[0021] (1) Graphene oxide modified polyether monomer: at 70-80°C, methallyl polyoxyethylene ether and graphene oxide react with p-toluenesulfonic acid for 5-8 hours to obtain modified permanent polyether monomer. Wherein the mass ratio of methallyl polyoxyethylene ether, graphene oxide and p-toluenesulfonic acid is: 100:7:4.
[0022] (2) Add the modified polyether monomer and water prepared in step (1) into the reactor to dissolve, put the reactor under ultraviolet light, and add the first solution and the second solution dropwise at a constant speed within 1-2h Carry out the polymerization reaction, after the dropwise addition, react at a constant temperature for 1 hour, add sodium hydroxide solution to neutralize to pH = 6-7, and obtain the enhanced polycarboxylate water reducer. Wherein the first solution is 2,2-dimethoxy-2-phenylacetophenone and 4-cyano-4-(phenylthioformylthio)valeric acid solution, and the second solution is maleic acid , N, N-dimethyl (meth)acrylamide ...
Embodiment 3
[0024] (1) Graphene oxide modified polyether monomer: At 70-80°C, isopentenyl polyoxyethylene ether and graphene oxide are reacted for 5-8 hours under the catalysis of p-toluenesulfonic acid to obtain modification Polyether monomer. Wherein the mass ratio of isopentenyl polyoxyethylene ether, graphene oxide and p-toluenesulfonic acid is: 100:10:3.
[0025] (2) Add the modified polyether monomer and water prepared in step (1) into the reactor to dissolve, put the reactor under ultraviolet light, and add the first solution and the second solution dropwise at a constant speed within 1-2h Carry out the polymerization reaction, after the dropwise addition, react at a constant temperature for 1 hour, add sodium hydroxide solution to neutralize to pH = 6-7, and obtain the enhanced polycarboxylate water reducer. Wherein the first solution is an aqueous solution of 4-hydroxybenzophenone and 2-(phenylthioformylthio)propionic acid, and the second solution is an aqueous solution of metha...
PUM
Property | Measurement | Unit |
---|---|---|
wavelength | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com