One-pot liquefaction process of biomass
A technology for biomass and pretreatment of biomass, applied in the field of one-pot liquefaction process of biomass, can solve the problems of unstable transportation, low amount of biomass conveyed by pumps, and high energy consumption, achieve volume reduction, avoid clogging, The effect of reducing industrial costs and energy consumption
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Embodiment 1
[0045] A one-pot liquefaction process of biomass, comprising the steps of:
[0046] Biomass Pretreatment
[0047] Put the palm oil residue into the drier and dry at 80°C for 5 hours until the water content is lower than 2wt%, and then send it into the superfine pulverizer for primary crushing. The median particle size after primary crushing is 100 μm, and then the primary crushing The palm oil residue is sent to the plodder for compression extrusion molding at a temperature of 50 °C and a pressure of 5 MPa, and then for secondary crushing. The median particle size after the secondary crushing is 30 μm. After the secondary crushing The bulk density of palm oil residue is 1600kg / m 3 ,spare.
[0048] Catalyst preparation
[0049] S1. After the biochar is acidified, a biochar carrier is obtained;
[0050] S2. Vibrating and grinding the oxide of Mo and the above-mentioned biomass carbon carrier to obtain the biomass carbon loaded with Mo oxide with a particle size of 400-500...
Embodiment 2
[0059] A one-pot liquefaction process of biomass, comprising the steps of:
[0060] Biomass Pretreatment
[0061] Send the linseed oil residue and peanut oil residue into a drier and dry at 110°C for 6 hours until the water content is lower than 2wt%, and then send them into an ultrafine pulverizer for primary crushing. The median particle size after primary crushing is 300 μm, and then The primary crushed linseed oil residue and peanut oil residue are sent to the plodder for compression extrusion molding at a temperature of 58°C and a pressure of 3MPa, and then secondary crushing is performed. The median particle size after the secondary crushing is 50 μm. The bulk density of linseed oil residue and peanut oil residue after secondary crushing is 1500kg / m 3 ,spare.
[0062] Catalyst preparation
[0063] S1. After the biochar is acidified, a biochar carrier is obtained;
[0064] S2. After the oxides of W, the oxides of Fe and the above-mentioned biomass charcoal carrier ...
Embodiment 3
[0073] A one-pot liquefaction process of biomass, comprising the steps of:
[0074] Biomass Pretreatment
[0075] Put saponin oil residue and rapeseed oil residue into a drier, dry at 100°C for 2 hours until the water content is lower than 2wt%, and then send it to an ultrafine pulverizer for primary crushing. The median particle size after primary crushing is 210 μm, Then the saponin oil residue and rapeseed oil residue after primary crushing are sent to a briquetting machine for compression extrusion molding at a temperature of 40°C and a pressure of 4MPa, and then secondary crushing is carried out. The particle size is 40 μm, and the bulk density of saponin oil residue and rapeseed oil residue after secondary crushing is 1561kg / m 3 ,spare.
[0076] Preparation of biochar loaded with Mo oxide and Pd oxide
[0077] S1. After the biochar is acidified, a biochar carrier is obtained;
[0078] S2. Vibrating and grinding Mo oxides, Pd oxides, and the above-mentioned biomass...
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