Polyester fiber with good antibacterial property
A polyester fiber, a good technology, applied in the field of polyester fiber, can solve the problems of huge harm, spread of pathogenic bacteria, etc., and achieve the effect of improving washability
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preparation example Construction
[0030] The preparation process of above-mentioned antibacterial agent A is:
[0031] S1. Zeolite modification:
[0032] First, the purchased natural zeolite was repeatedly washed with distilled water, filtered and dried at 100°C for 12 hours;
[0033] Then, add hydrochloric acid, potassium hydroxide, sodium chloride solution in the flask, add distilled water again and dilute to 80ml, control hydrochloric acid, potassium hydroxide, sodium chloride concentration to be 0.5, 0.4, 0.9mol / L respectively, add 8.9g zeolite , heated in a water bath, stirred at a constant speed at 94°C for 6h, washed with distilled water until Cl-free - residue, and then calcined at 100°C for 12 hours to obtain a modified zeolite;
[0034] S2, prepare antibacterial agent A
[0035] Mix tetrabutyl titanate, absolute ethanol, and nitric acid at a volume ratio of 6:24:1, add calcium chloride powder, and control the doping of metal calcium ions on TiO 2 The mass fraction in is 1.7wt.%, magnetically stir...
Embodiment 1
[0059] In this example, a kind of polyester fiber with good antibacterial performance is mixed with antibacterial agent A and antibacterial agent B to form a mixed antibacterial agent, and then pure PET slices are blended with the mixed antibacterial agent to prepare antibacterial modified PET slices, and then passed Polyester fibers with good antibacterial properties were obtained by melt spinning.
[0060] The above-mentioned polyester fibers include: 0.7wt.% of antibacterial agent A, 0.3wt.% of antibacterial agent B, and the balance of polyester fiber according to weight percentage.
[0061] Wherein, the antibacterial agent A is TiO prepared by gel-sol method 2 / Zeolite antibacterial agent, zeolite as carrier, TiO 2 doped with metallic Ca 2+ ion. TiO 2 / zeolite in the TiO 2 The loading amount is 35wt.%, Ca 2+ ions in TiO 2 The doping mass fraction is 1.7wt.%.
[0062] The antibacterial agent B is Cu prepared by gel-sol method 2 O / zeolite antibacterial agent, zeoli...
Embodiment 2
[0065] In this example, a kind of polyester fiber with good antibacterial performance is mixed with antibacterial agent A and antibacterial agent B to form a mixed antibacterial agent, and then pure PET slices are blended with the mixed antibacterial agent to prepare antibacterial modified PET slices, and then passed Polyester fibers with good antibacterial properties were obtained by melt spinning.
[0066] The above polyester fibers include: 1.0wt.% of antibacterial agent A, 0.5wt.% of antibacterial agent B, and the rest of polyester fiber according to weight percentage.
[0067] Wherein, the antibacterial agent A is TiO prepared by gel-sol method 2 / Zeolite antibacterial agent, zeolite as carrier, TiO 2 doped with metallic Ca 2+ ion. TiO 2 / zeolite in the TiO 2 The loading amount is 35wt.%, Ca 2+ ions in TiO 2 The doping mass fraction is 1.7wt.%.
[0068] The antibacterial agent B is Cu prepared by gel-sol method 2 O / zeolite antibacterial agent, zeolite as carrier...
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