Greases for elevator slings, elevator slings and traction elevators
A grease, sling technology, applied in lubricating compositions, textile cables, transportation and packaging, etc., can solve problems such as pressure rise, wear increase, sling load increase, etc.
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[0126] Hereinafter, the present invention will be specifically described using examples and comparative examples, but the present invention is not limited to these examples.
[0127] (1) Evaluation method of slime oil and grease
[0128] (1-1) Determination of Sports viscosity, consistency and dropout of slime oil
[0129] Sports viscosity (40 ° C, 100 ° C) was determined based on JIS standards (JIS K2283). Further, the consistency of the grease (no mixed consistency, mixing consistency) and droppoint are determined based on the JIS standard (JIS K2220). In addition, the viscosity level is evaluated based on the value of the movement viscosity of the slim oil, based on ISO (International Organization for Standardization, International Standardization) 3448.
[0130](1-2) Determination of traction coefficient
[0131] Traction coefficient measurement is carried out using a Ball on disk (ball) test device. This test device has a mechanism that rotates between the ball and the bilate...
reference example 7
[0183] (2-10) Reference Example 7: Synthesis of Synthetic Oil 11
[0184] Typete olene 1 kg, cyclohexane 200 ml, 1,2-diethoxyethane 100 ml and a cation exchange resin 100 g as a catalyst were added to 60 ° C for 6 hours at 60 ° C for 6 hours. After the reaction, cooled with a water bath at 20 ° C, and the solid catalyst was filtered. The reaction solution is added to the 1L autoclave by the rotary evaporator, 500 g of the reaction liquid is added to the 1L autoclave, and the nickel catalyst for hydrogenation is added, and after seating, it is 50 kg / cm by hydrogen pressure. 2 (G), 120 ° C for 4 hours to hydrogenate, naturally cooled to room temperature, and filter out the catalyst.
[0185] The resulting product was analyzed by gel filtration chromatography, resulting in the formation of dimer components (synthetic oil 11). Decompression distillation was performed on the total reaction mixture and only the dimer component was separated.
[0186] (2-11) Reference Example 8: Synthe...
Embodiment 1
[0191] Examples 17 to 26 modify the synthetic oil of Example 1 to other polycyclic alkane compounds (synthetic oils 6 to 15). The composition and evaluation results of the base oil are shown in Table 4. The high traction coefficient and wear resistance were displayed in the same manner as in Example 1.
[0192] [Table 4]
[0193]
[0194] (2-14) Reference Example 9: Production of Thickeners
[0195] In a 3 L of the glass reactive container, 300 g of ethylenediamine 30g and 12-hydroxyglyctaryic acid were dissolved in meta xylene, and 15 g of ferric chloride (III) (III) hexahydrate as a catalyst was added, and heated and refluxed for 10 hours. After filtering out the product, the product was separated and refined by recrystallization.
[0196] The resulting product was analyzed by gel filtration chromatography, resulting in a fatty acid diamine (N, N'-ethylene-dibly-12-hydroxy stetonlamide).
[0197] (2-15) Examples 27 to 33 and Comparative Example 2 of the production and evaluati...
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