Preparation method for grouting material
A technology of grouting material and mixture, which is applied in the field of grouting material preparation, which can solve the problems of easy shrinkage, poor bonding performance of grouting material, single distribution, etc., to increase bearing area, increase bonding performance, and increase crosslinking density Effect
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[0021] A preparation method for grouting material, comprising the steps of:
[0022] (1) Take polyethylene glycol 200 and mix it with glycerin at a mass ratio of 8:3 to obtain a mixture. Take the mixture and add starch at a mass ratio of 6:1, then add methanesulfonic acid with a mass ratio of 3 to 5% of the mixture, and heat up to 140~ Stir and mix at 150°C for 2~3h, cool to 60~80°C to obtain a cooled product, take the cooled product and add 10% sodium hydroxide solution with a mass fraction of 5:2, stir and mix for 20~30min to obtain a stirred mixture;
[0023] (2) Take the stirred mixture and raise the temperature to 110~115°C, vacuum dehydrate at -0.09~-0.1MPa for 2~3h, cool to 50~60°C, and add 50~70% of the mass of the stirred mixture to diphenyl Methane diisocyanate, stirred and mixed at 75~80°C for 3~4h to obtain mixture A, in parts by mass, take 20~30 parts of mixture A, 12~15 parts of hydroxypolydimethylsiloxane, 50~70 parts Acetone, 2~5 parts of N,N-dimethylcyclohexy...
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