A kind of medical polyurethane elastomer with biocompatibility and preparation method thereof
A technology of polyurethane elastomer and biocompatibility, applied in the field of polyurethane elastic fibers, can solve the problems of difficulty in obtaining polyurethane elastic fibers with heat resistance, uniformity of filaments, not being widely promoted, insufficient mechanical properties and uniformity, etc. Achieve the effect of avoiding adverse effects, excellent biocompatibility, long-term application
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[0038] A kind of medical polyurethane elastic fiber with biocompatibility and preparation method thereof of the present invention, its preparation steps are as follows:
[0039] 1.) Preparation of polyurethane slices: Add polyglycol, aliphatic diisocyanate A, chain-extending diol, catalyst, auxiliary materials, etc., after metering, directly into the twin-screw reactor for melting, mixing, and slicing to obtain polymer P1, after the cleaning process, vacuum-dry at 90-100°C, and wait for the next step to use;
[0040] 2.) Preparation of modified prepolymer: Mixing and reacting modified aliphatic diisocyanate A' with polyglycol to generate prepolymer P2, which is protected by dry nitrogen;
[0041] 3.) Melt and extrude the polymer P1 and the prepolymer P2 at a ratio of 19:1 to 3:1 and fully mix it in a static mixer, then pass through the melt metering pump, the distribution plate to the spinneret;
[0042] 4.) Through the spinning box, side blowing cooling device, spinning tunn...
Embodiment 1
[0044] 1.) Polytetrahydrofuran-caprolactone diol (PTMEG-PCL) with 1.00mol molecular weight of 2000, 1.05mol 1,4-cyclohexane diisocyanate, 1.00mol ethylene glycol, catalyst, 1% antioxidant, Add 0.5% ultraviolet absorber, 0.5% anti-yellowing agent, 1% anti-hydrolysis stabilizer, etc. directly into the twin-screw reactor for melting, mixing, and slicing to obtain polymer P1. Vacuum dried, ready to use;
[0045] 2.) Preparation of modified aliphatic diisocyanate: blend 1.0 g of chlorhexidine acetate, 1.0 g of heparin and 100.0 g of 1,4-cyclohexane diisocyanate, and stir evenly to obtain modified aliphatic diisocyanate A';
[0046] 3.) Mix and react 1.00mol modified aliphatic diisocyanate A' with 1.05mol polytetrahydrofuran-caprolactone diol to generate prepolymer P1, which is protected with dry nitrogen;
[0047] 4.) Melt and extrude the polymer P1 and the prepolymer P2 at a ratio of 85 / 15 and fully mix it in a static mixer, then pass through the melt metering pump, and then dist...
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