Preparation method of non-ironing finishing agent for chemical fiber fabric

A non-iron finishing and fabric technology, which is applied in fiber treatment, textiles and papermaking, etc., can solve the problems of affecting the wearing comfort of fabrics, the decrease of fabric strength, and poor moisture absorption and air permeability, so as to ensure moisture absorption and air permeability, enhance porosity, and enhance Infiltrating effect

Inactive Publication Date: 2018-10-09
ANHUI HENGYI TEXTILE TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

After non-iron finishing, the strength of the fabric decreases significantly, the hand feels hard, and the moisture absorption and

Method used

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  • Preparation method of non-ironing finishing agent for chemical fiber fabric

Examples

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Comparison scheme
Effect test

Embodiment 1

[0028] A preparation method for a non-ironing finishing agent for chemical fiber fabrics, comprising the following steps:

[0029] (1) Put 50 parts of polyester polyurethane into a ball mill and mill it for 80 minutes at a rotating speed of 280r / min. After ball milling, clean it with ethanol and put it into a vacuum drying oven to dry. Among them, zirconia balls are used for ball milling, and the ball-to-material ratio is 1.2:1;

[0030] (2) Mix 100 parts of acrylic acid, 25 parts of bisphenol A epoxy resin, 5 parts of fatty acid diethanolamide and 20 parts of polyparabenamide, put them in a vacuum oven at 90°C for 5 hours, cool and grind, Go through a 120-mesh sieve, put it into an ultrasonic instrument, and ultrasonicate it for 20 minutes under the condition of 60KHz and 150W, wash it with ethanol, put it into a vacuum drying oven to dry, then transfer it to a magnesium chloride solution with a mass concentration of 3%, and ultrasonicate it for 20 minutes under the condition...

Embodiment 2

[0034] A preparation method for a non-ironing finishing agent for chemical fiber fabrics, comprising the following steps:

[0035] (1) Put 60 parts of polyester polyurethane into a ball mill and mill at 240r / min for 90min. After ball milling, wash with ethanol and dry in a vacuum drying oven. Zirconia balls are used for ball milling, and the ball-to-material ratio is 1.3:1;

[0036] (2) Mix 150 parts of acrylic acid, 45 parts of bisphenol-A epoxy resin, 8 parts of fatty acid diethanolamide and 25 parts of polyparabenamide, put them in a vacuum oven at 95°C for 6 hours, cool and grind, Pass through a 120-mesh sieve, put it into an ultrasonic instrument, and ultrasonicate it for 25 minutes under the condition of 60KHz and 150W, wash it with ethanol, put it into a vacuum drying oven to dry, and then transfer it to a magnesium chloride solution with a mass concentration of 4%, and ultrasonicate it for 10 minutes under the condition of 60KHz and 150W. Wash with deionized water and...

Embodiment 3

[0043] A preparation method for a non-ironing finishing agent for chemical fiber fabrics, comprising the following steps:

[0044] (1) Put 70 parts of polyester polyurethane into a ball mill and ball mill for 85 minutes at a speed of 300r / min. After ball milling, use ethanol to clean it, and put it into a vacuum drying oven to dry. Among them, zirconia balls are used for ball milling, and the ball-to-material ratio is 1.2:1;

[0045] (2) Mix 120 parts of acrylic acid, 30 parts of bisphenol A epoxy resin, 6 parts of fatty acid diethanolamide and 22 parts of polyparabenamide, put them in a vacuum drying oven at 100°C for 5 hours, cool and grind, Go through a 120-mesh sieve, put it into an ultrasonic instrument, and ultrasonicate it for 30 minutes under the condition of 60KHz and 150W, wash it with ethanol, put it into a vacuum drying oven to dry, then transfer it to a magnesium chloride solution with a mass concentration of 5%, and ultrasonicate it for 20 minutes under the condi...

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Abstract

The invention discloses a preparation method of a non-ironing finishing agent for chemical fiber fabric, and relates to the technical field of processing of chemical fiber fabric. The preparation method of the non-ironing finishing agent for the chemical fiber fabric comprises the following steps: (1) putting polyester type polyurethane into a ball mill and performing ball milling; (2) mixing acrylic acid, bisphenol A type epoxy resin, fatty acid diethanolamide and poly(p-phenylformamide) uniformly, performing ultrasonic treatment, shifting to a magnesium chloride solution, performing ultrasonic treatment, cleaning and drying; (3) mixing benzoyl peroxide, sucrose fatty acid ester and pentaerythritol fatty acid ester uniformly, sintering, cooling and performing treatment under saturated vapor pressure; (4) mixing the prepared mixtures uniformly, adding into a mixed solution of ethanol and water, adding sodium sulphite, sodium secondary alkyl sulfate and ammonium hydrogen carbonate, mixing uniformly and adjusting PH to prepare the non-ironing finishing agent. The non-ironing finishing agent can achieve the non-ironing effect, can maintain the original strength, hand feeling comfortability as well as moisture absorbing and air-permeable properties of the chemical fiber, and guarantees the wearing comfortability.

Description

Technical field: [0001] The invention relates to the technical field of chemical fiber fabric processing, in particular to a preparation method for a non-ironing finishing agent for chemical fiber fabrics. Background technique: [0002] Cellulose fiber fabrics are more and more popular due to their good hygroscopicity and wearing comfort. However, due to its own characteristics, cellulose fibers are prone to wrinkling, unevenness and unsightly appearance during wearing and washing. Therefore, after each washing, ironing is required to keep it smooth and crisp, which brings great benefits to people's daily life. A lot of inconvenience came. In order to overcome this shortcoming, people improve by carrying out non-ironing processing to fabric. The usual method is to first impregnate the entire fabric with resin on the tenter frame, and then bake it at a high temperature of 130°C-160°C or stack it at normal temperature to achieve the purpose of non-ironing. After non-ironing...

Claims

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Application Information

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IPC IPC(8): D06M15/572D06M11/54D06M11/76D06M13/203D06M13/224D06M15/55D06M15/59
CPCD06M11/54D06M11/76D06M13/203D06M13/224D06M15/55D06M15/572D06M15/59
Inventor 李贺
Owner ANHUI HENGYI TEXTILE TECH CO LTD
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