High-resilience closed flame-retardant foam silicon rubber material and preparation method thereof
A technology of flame-retardant foam and silicone rubber, which is applied in the field of high-resilience closed-cell flame-retardant silicone rubber foam and its preparation, and can solve the problem of reducing the shock absorption performance of silicone rubber foam, uneven cell size, and enlarged cells. problem, achieve the effect of reducing cell size, optimizing cell distribution, and reducing cell diameter
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[0030] The present invention also provides a preparation method of a high-resilience closed-cell flame-retardant foamed silicone rubber material, which comprises the following steps:
[0031] Step 1. Add 40-60% of silicone rubber, 30-50% of additives, 0.5-2% of foaming agent, 0.5-2% of catalyst, 0.5-2% of inhibitor, and 0.5-1.5% of colorant into the planet by weight percentage In the stirrer, vacuumize and mix at 110°C-160°C for 30-40min, and let the mixture return to room temperature;
[0032] Step 2. Add 1~3% of crosslinking agent to the mixture in the planetary mixer, turn on the cold circulation system, control the temperature at 5°C-10°C, and quickly mix and stir for 10-20 minutes until the mixture is uniform to obtain the spare rubber;
[0033] Step 3: Cover the upper and lower parts of the spare rubber obtained in Step 2 with a layer of polyester film and calender through a double-roller calender, and then enter a high-temperature oven through a conveyor belt, and perfo...
Embodiment 1
[0037]Step 1. Add 40% of silicone rubber, 50% of additives, 2% of foaming agent, 2% of catalyst, 2% of inhibitor and 1% of coloring agent into the planetary mixer by weight percentage, and vacuumize and mix at 110°C for 40 min, let stand until the mixture returns to room temperature;
[0038] Step 2: Add 3% cross-linking agent to the mixture in the planetary mixer, turn on the cold circulation system, control the temperature at 5°C, and quickly mix and stir for 20 minutes until the mixture is evenly mixed to obtain the spare rubber;
[0039] Step 3: Cover the upper and lower parts of the spare rubber obtained in Step 2 with a layer of polyester film and calender through a double-roller calender, and then enter a high-temperature oven through a conveyor belt, and perform normal pressure foaming and vulcanization at 60°C for 15 minutes. The continuous foamed silica gel sheet is rolled to obtain a high-resilience closed-cell flame-retardant foamed silicone rubber material coil. ...
Embodiment 2
[0041] Step 1. Add 60% of silicone rubber, 30% of additives, 2% of foaming agent, 2% of catalyst, 2% of inhibitor, and 1% of coloring agent into the planetary mixer by weight percentage, and vacuumize and mix at 160°C for 30 min, let stand until the mixture returns to room temperature;
[0042] Step 2. Add 3% crosslinking agent to the mixture in the planetary mixer, turn on the cold circulation system, control the temperature at 10°C, and mix and stir quickly for 10 minutes until the mixture is evenly mixed to obtain the spare rubber;
[0043] Step 3: Cover the upper and lower parts of the spare rubber obtained in Step 2 with a layer of polyester film and calender through a double-roller calender, then enter a high-temperature oven through a conveyor belt, and perform normal-pressure foaming and vulcanization at 120°C for 5 minutes to form The continuous foamed silica gel sheet is rolled to obtain a high-resilience closed-cell flame-retardant foamed silicone rubber material co...
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