A Modified Zirconium Silicate Whisker Reinforced Alumina Ceramics
A technology of zirconium silicate whiskers and alumina ceramics, which is applied in the field of modified zirconium silicate whiskers to reinforce alumina ceramics, can solve problems such as brittleness limitation, achieve dispersion stress, improve ceramic wear resistance, and increase compactness Effect
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Embodiment 1
[0022] A modified zirconium silicate whisker-reinforced alumina ceramic, the modified zirconium silicate whisker-reinforced alumina ceramic contains 6.40% of its mass modified zirconium silicate whisker and 3.20% of mercapto-nano-hybrid Material.
[0023] Further, the preparation method of the modified zirconium silicate whiskers is:
[0024] (1) Pretreatment: Prepare sodium iron chromium lignosulfonate into an aqueous solution with a mass concentration of 6.3%, then add zirconium silicate whiskers, stir evenly, heat to 50°C, and then gradually add dropwise with a mass concentration of 5% Hydrogen peroxide was kept at 50°C in a water bath for 2 hours, then filtered, washed with deionized water, and dried to constant weight to obtain pretreated zirconium silicate whiskers;
[0025] (2) Modifier preparation: Add deionized water to the reactor, then add phosphoric acid and N,N-dimethylacetamide to the reactor, heat to 88-90°C, and stir at 350r / min for 30min , and then add nano-...
Embodiment 2
[0037] A modified zirconium silicate whisker reinforced alumina ceramic, the modified zirconium silicate whisker reinforced alumina ceramic contains 6.46% of its mass modified zirconium silicate whisker and -3.23% of mercapto-containing nano-doped material.
[0038] Further, the preparation method of the modified zirconium silicate whiskers is:
[0039] (1) Pretreatment: Prepare sodium iron chromium lignosulfonate into an aqueous solution with a mass concentration of 6.3%, then add zirconium silicate whiskers, stir evenly, heat to 50°C, and then gradually add dropwise with a mass concentration of 5% Hydrogen peroxide was kept at 50°C in a water bath for 2 hours, then filtered, washed with deionized water, and dried to constant weight to obtain pretreated zirconium silicate whiskers;
[0040] (2) Modifier preparation: Add deionized water to the reactor, then add phosphoric acid and N,N-dimethylacetamide to the reactor, heat to 88-90°C, and stir at 350r / min for 30min , and the...
Embodiment 3
[0052] A modified zirconium silicate whisker reinforced alumina ceramic, the modified zirconium silicate whisker reinforced alumina ceramic contains 6.44% of its mass modified zirconium silicate whisker and 3.22% of mercapto-nano-hybrid Material.
[0053] Further, the preparation method of the modified zirconium silicate whiskers is:
[0054] (1) Pretreatment: Prepare sodium iron chromium lignosulfonate into an aqueous solution with a mass concentration of 6.3%, then add zirconium silicate whiskers, stir evenly, heat to 50°C, and then gradually add dropwise with a mass concentration of 5% Hydrogen peroxide was kept at 50°C in a water bath for 2 hours, then filtered, washed with deionized water, and dried to constant weight to obtain pretreated zirconium silicate whiskers;
[0055] (2) Modifier preparation: Add deionized water to the reactor, then add phosphoric acid and N,N-dimethylacetamide to the reactor, heat to 88-90°C, and stir at 350r / min for 30min , and then add nano-...
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