Preparation method of zinc nitride composite thin film with improved properties
A composite film and zinc nitride technology, applied in the field of layered materials, can solve the problems of increased leakage current and achieve the effects of reduced power consumption, low manufacturing cost, and low frequency of use
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[0018] figure 1 It is a flow chart of the preparation method of the zinc nitride composite film according to the present invention. As shown in the figure, the preparation method of the present invention includes the following steps:
[0019] Step 101: preparing a monocrystalline silicon substrate with a clean surface;
[0020] Step 102: Deposit a first ZnO layer on the surface of the single crystal silicon substrate using the first magnetron sputtering process parameters, wherein the thickness of the first ZnO layer is 10-15 nm;
[0021] Step 103: Deposit a metal Zn layer on the surface of the first ZnO layer with the second magnetron sputtering process parameters, wherein the thickness of the metal Zn layer is 5-10 nm;
[0022] Step 104: deposit a second ZnO layer on the surface of the metal Zn layer using the third magnetron sputtering process parameters, wherein the thickness of the second ZnO layer is 20-30 nm;
[0023] Step 105: Deposit a first AZO layer on the surface of the se...
Embodiment 1
[0029] The zinc nitride-based composite film material is prepared by the following method: prepare a single crystal silicon substrate with a clean surface; deposit a first ZnO layer on the surface of the single crystal silicon substrate with the first magnetron sputtering process parameters, wherein the first ZnO layer The thickness of the metal Zn layer is 10nm; the metal Zn layer is deposited on the surface of the first ZnO layer with the second magnetron sputtering process parameters, wherein the thickness of the metal Zn layer is 5nm; the metal Zn layer is deposited with the third magnetron sputtering process parameters The second ZnO layer, wherein the thickness of the second ZnO layer is 20nm; the first AZO layer is deposited on the surface of the second ZnO layer with the fourth magnetron sputtering process parameters, wherein the thickness of the first AZO layer is 25nm; A second AZO layer was deposited on the surface of an AZO layer with the fifth magnetron sputtering p...
Embodiment 2
[0031] The zinc nitride-based composite film material is prepared by the following method: prepare a single crystal silicon substrate with a clean surface; deposit a first ZnO layer on the surface of the single crystal silicon substrate with the first magnetron sputtering process parameters, wherein the first ZnO layer The thickness of the metal Zn layer is 15nm; the metal Zn layer is deposited on the surface of the first ZnO layer with the second magnetron sputtering process parameters, wherein the thickness of the metal Zn layer is 10nm; the metal Zn layer is deposited with the third magnetron sputtering process parameters The second ZnO layer, wherein the thickness of the second ZnO layer is 30nm; the first AZO layer is deposited on the surface of the second ZnO layer with the fourth magnetron sputtering process parameters, wherein the thickness of the first AZO layer is 40nm; A second AZO layer was deposited on the surface of an AZO layer with the fifth magnetron sputtering ...
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