58 results about "Zinc nitride" patented technology

A deposition technique for forming an oxynitride film is provided. A highly reliable semiconductor element is manufactured with the use of the oxynitride film. The oxynitride film is formed with the use of a sputtering target including an oxynitride containing indium, gallium, and zinc, which is obtained by sintering a mixture of at least one of indium nitride, gallium nitride, and zinc nitride as a raw material and at least one of indium oxide, gallium oxide, and zinc oxide in a nitrogen atmosphere. In this manner, the oxynitride film can contain nitrogen at a necessary concentration. The oxynitride film can be used for a gate, a source electrode, a drain electrode, or the like of a transistor.

The invention relates to a metal surface treatment passivation liquid which comprises 1-20g/L zinc nitride, 5-40g/L inorganic acid, a 5-50g/L dispersant and a 1-10g/L modified mesoporous nano material. The modified mesoporous nano material is a polybasic acid grafted mesoporous nano material, and the percent grafting of polybasic acid is 1-5wt%. A film with extremely good corrosion resistance andadhesive force is obtained on the metal surface treated by the passivation liquid.

The invention discloses a method for preparing a P-type zinc oxide film from in situ low-pressure oxidized aluminum-doped zinc nitride; an ultra-high vacuum magnetron sputtering system is adopted to prepare an aluminum-doped zinc nitride film on a quartz substrate as a precursor, wherein the select purity of a target is 99.999 percent high-purity zinc; and a high-purity aluminum sheet is put on the surface of the target to control the aluminum content in a sample. After the precursor is prepared, the background of a reaction chamber is vacuumized to be 10 to 4Pa, and 99.999 percent high-purity oxygen is fed in to oxidize the precursor at low pressure. The method improves the active nitrogen content in the zinc oxide with nitrogen and aluminum doping, improves the concentration and the mobility of a hole carrier, and reduces the resistivity of the zinc oxide film. When the oxidation temperature is 550DEG C, the resistivity is low to 19.8(ohm.cm), the concentration of the carrier reaches +4.6E1018cm-3. An optical band gap is 3.27Ev, and the film has excellent crystalline state and optical properties.

The invention provides a method for preparing a nitrogen aluminum co-doping p type zinc oxide thin film. The method comprises the following steps that S1, high-purity zinc serves as a target material, a high-purity aluminum piece is placed on the target face, a substrate is placed above the target material, the distance between the substrate and the target material is adjustable, high-purity nitrogen gas is led to carry out radio frequency magnetron reactive sputtering, and the aluminum-contained zinc nitride thin film obtained through preparation serves as a precursor; S2, after the precursor is prepared, vacuumizing is carried out, high-purity oxygen is led to carry out in-situ low-pressure oxidization on a precursor thin film, and the nitrogen aluminum co-doping p type zinc oxide thin film is obtained through preparation. According to the method, on the premise that the performance of the precursor is optimized, the content of active nitrogen in the thin film is improved, and therefore the concentration and the migration rate of a hole carrier are increased, the resistance rate of the zinc oxide thin film is reduced, the resistance rate of the obtained zinc oxide thin film is reduced to 10.84W*cm, the concentration of the carrier reaches +4.65*1018cm-3, an optical band gap is 3.27 eV, and the crystalline state and the optical property of the thin film are good.

The invention discloses a zinc nitride and copper nitride compound of chiral alpha-phenylethylamine, which comprises a (S) alpha-phenylethylamine zinc nitride and copper nitride compound and a (R) alpha-phenylethylamine zinc nitride and copper nitride compound, which are prepared from the alpha-phenylethylamine, zinc acetate dihydrate, copper acetate monohydrate and copper chloride dihydrate and have the following formulas. In the formulas, ML is Zn(OOCCH3)2, Cu(OOCCH3)2 or CuCl2. The compound serves as a chiral catalyst in a Henry reaction.

To provide a semiconductor memory device having a floating gate which operates with a short channel. A high-work-function compound semiconductor having a work function of greater than or equal to 5.5 eV, such as indium nitride or zinc nitride, is used for the floating gate. Accordingly, the potential barrier of the floating gate insulating film between the substrate and the floating gate is higher than that of a conventional one, so that leakage of electric charge due to a tunnel effect can be reduced even if the thickness of the floating gate insulating film is made small. Since the thickness of the floating gate insulating film can be made small, the channel can be further shortened.

The invention discloses a method for preparing a nitrogen oxygen zinc thin film. Radio frequency magnetron sputtering is used, a zinc nitride target which is 99.9-99.999% in volume percentage is taken as sputtering target materials, and the distance between the target materials and a substrate is 20-150mm; under certain radio frequency, argon which is 99.9-99.999% in volume percentage is taken as sputtering gas, sputtering is carried out at the substrate temperature of 25-150DEG C and at power density of 0.5-5W/cm2, and the background vacuum of a sputtering room is smaller than 1*10-7torr; pre-sputtering is carried out for a period of time through the argon, and then oxygen which is 99.9-99.999% in volume percentage is taken as reaction gas to obtain the nitrogen zinc oxide thin film with oxygen flow of 0.1-60sccm and argon flow of 5-100sccm and at sputtering pressure of 0.1-10.0Pa, wherein the atomic number of Zn accounts for 51-66%, and N:O=1:3-2:1. The method for preparing the nitrogen zinc oxide thin film solves the problem that the nitrogen is low in solid solubility in zinc oxide, and the prepared n-type nitrogen zinc oxide thin film is high in carrier mobility and low in specific resistance.

Embodiments disclosed herein relate to a TFT and methods for manufacture thereof. Specifically, the embodiments herein relate to methods for forming a semiconductor layer at a low temperature for use in a TFT. The semiconductor layer may be formed by depositing a nitride or oxynitride layer, such as zinc nitride or oxynitride, and then converting the nitride layer into an oxynitride layer with a different oxygen content. The oxynitride layer is formed by exposing the deposited nitride layer to a wet atmosphere at a temperature between about 85 degrees Celsius and about 150 degrees Celsius. The exposure temperature is lower than the typical deposition temperature used for forming the oxynitride layer directly or annealing, which may be performed at temperatures of about 400 degrees Celsius.

Provided are fluorine-containing zinc targets, methods of fabricating a zinc oxynitride thin film by using the zinc targets, and methods of fabricating a thin film transistor by using the zinc oxynitride thin film. The methods include mounting a fluorine-containing zinc target and a substrate in a sputtering chamber, supplying nitrogen gas and inert gas into the sputtering chamber, and forming a fluorine-containing zinc oxynitride thin film on the substrate.

The invention relates to a surface anticorrosion method for neodymium iron boron ferrite. The surface anticorrosion method for neodymium iron boron ferrite comprises the steps of firstly, carrying out pretreatment, carrying out treatment of oil removal, polishing, rinsing, activation, second time of rinsing and the like on the neodymium iron boron ferrite so as to guarantee that the outer surface of the neodymium iron boron ferrite is clean and smooth; secondly, injecting the anticorrosion material zinc nitride onto the surface of the neodymium iron boron ferrite in an ion injection manner; and carrying out passivation treatment on the surface of the neodymium iron boron ferrite.

The invention discloses a preparation method of a polycrystalline zinc nitride film, belonging to the technical field of electronic materials, characterized in that: a polycrystalline Zn3N2 film is prepared at room temperature by reactive radio-frequency magnetron sputtering on a quartz substrate, the sputtering target is a pure metal Zn target, the distance between the sputtering target and the substrate is 50-80 mm, the basic vacuum of a sputtering chamber is less than 1.0*10<-3> Pa, the sputtering gas is argon, the reactive gas is ammonia, the flow range of the ammonia is 1-5 sccm, the flow range of the argon is 15-19 sccm, and the total flow of the argon and the ammonia is 20 sccm; the pressure intensity of the argon-ammonia mixed gas in the sputtering chamber is 0.5-2.5 Pa, the radio-frequency sputtering power is 30-200 w, and the temperature of the substrate is room temperature. The invention has the advantages of low cost, convenient preparation of target material, recycle target material, and no need of heating the substrate, and the prepared polycrystalline zinc nitride film has large optical band gap.

The invention belongs to the technical field of textile auxiliary agents and discloses a wetting agent as well as a preparation method and application of the wetting agent. The wetting agent is prepared from the following components in parts by weight: 1 to 1.2 parts of trans-4-[(2-amino-3,5-dibromobenzyl)amino]cyclohexanol, 3 to 5 parts of citric acid triamine, 0.1 to 0.5 part of methyl orange, 12 to 14 parts of sodium sulfate, 0.5 to 0.7 part of zinc nitride, 3 to 4 parts of sodium dimethylbenzenesulfonate, 0.6 to 0.9 part of methylisothiazolinone, 100 to 120 parts of polyethylene glycol and 300 to 350 parts of de-ionized water. The invention also discloses the preparation method of the wetting agent. The wetting agent disclosed by the invention can be widely applied to a plurality of processes of sizing, bleaching, desizing, refining, dyeing, after-finishing textiles and the like, can be used for mercerization treatment on pure cotton textiles and carbonization treatment on wool textiles, and has a wide application prospect.

The invention provides an assistant for improving the heat absorption performance of a PET polyester chip and a production method of a PET bottle. According to the assistant for improving the heat absorption performance of the PET polyester chip and the production method of the PET bottle, titanium nitride or zinc nitride is added into the assistant to form a mixed assistant, so the heat absorption performance of the PET polyester chip is more uniform; in addition, the color of titanium nitride/zinc nitride is more close to light blue compared with a traditional carbon black heat absorber, so compared with a traditional carbon black heat absorption additive chip, the chip of the invention has the advantages of higher L value, lower b value, higher transparency and higher degree of fineness; and comprehensive cost is lower, and 30%-50% of raw material cost is saved for manufacturers.

The invention discloses anticorrosive coating for LED lamps. The anticorrosive coating comprises the following raw materials in parts by mass: 20-30 parts of waterborne acrylic resin, 10-20 parts of fluorosiloxane, 5-15 parts of zinc nitride, 1-2.5 parts of glass fiber, 5-12 parts of kaolin, 10-15 parts of far infrared ceramic nanoparticles, 1-5 parts of gaseous titanium dioxide, 10-30 parts of asolvent, 0.5-1.5 parts of a wetting and dispersing agent, 2-3 parts of an MOK-2015 leveling agent and 15-25 parts of a curing agent, wherein the solvent is a mixture of glycerol, coconut oil and ethylformate; the wetting and dispersing agent is the MOK-2030 dispersing agent; the curing agent is a waterborne isocyanate curing agent; the glass fiber is sodium calcium glass fiber with the particle size of 50-150 nm; and the sizes of the far infrared ceramic nanoparticles are 100-150 nm. Coating formed by the anticorrosive coating has excellent mechanical properties and a protective function, andalso has good waterproof and anticorrosive characteristics while radiating temperature reduction is achieved; and the anticorrosive coating is simple and convenient in production process and convenient to use.

This invention relates to a preparation method of film materials of acceptor Zn oxide obtaining P-type Zn oxide material by high temperature thermal-oxidating Zn nitride single crystal film to control the acceptor impurity concentration of type-P Zn oxide material by controlling oxidation temperature and thermal-oxidative time. Nitride in cubic antiferro Mn ore is easy to be substituted by oxygen under high temperature and form hexagonal P-type Zn oxide, realizing nitride doped substitution to from P-type Zn oxide and process its film materials with the accepter concentration of 6X10 to the power 16 - 4X10 to the power 18 cm to the power -3 and hexagonal P-type Zn oxide film material, realizing control of Zn oxide electricity performance and carrier concentration which Satifies the needs of preparing P-N material of Zn oxide and photo electronic apparatus.

The invention discloses a preparation method and device for biomass fast-burning bricks. The preparation method is to add sodium bicarbonate, potassium permanganate, zeolite powder, sodium silicate and fatty alcohol polyoxygen after drying the biomass to remove impurities. Sodium vinyl ether sulphate, mixed evenly, the intermediate product is obtained through two heating reactions, then add water, zinc nitrate, calcium oxide, bentonite, epoxy resin, gum arabic and xanthan gum, mix evenly, heat up and extrude , to obtain biomass fast-burning bricks. The device provided by the invention comprises a drying unit, a mixing unit, a reaction unit, a pulverizing unit and an extruding unit connected in sequence, and the connection between the units is through a conveyor belt. The biomass quick-combustible brick obtained by the preparation method provided by the invention is easy to ignite when used, has a fast burning speed and is fully burned, and does not emit dust and other pollutants to the surroundings. The preparation process of the device provided by the invention can be fully automated and controlled, and the preparation efficiency is high.

The invention discloses a corrosion-resistant metal ceramic material and a preparation method thereof. The corrosion-resistant metal ceramic material comprises, by weight, 18-25 parts of copper oxide, 15-20 parts of silicon dioxide, 10-20 parts of graphite, 10-15 parts of zinc nitride, 5-10 parts of nickel, 5-10 parts of molybdenum oxide, 5-10 parts of teflon, 3-5 parts of sodium tripolyphosphate and 0.1-1 part of tributyl tin methacrylate. The corrosion-resistant metal ceramic material has strong corrosion resistance, raw materials are easy to obtain, and the cost of the raw materials is low; the production process is simple, and the production cost is reduced; and in addition, the corrosion-resistant metal ceramic material has the advantages of being short in production cycle and good in high temperature resistance.

The invention belongs to the technical field of complex motor cases, in particular to a casting method capable of preventing deformation of a complex motor case. The casting method capable of preventing deformation of the complex motor case comprises processes of melt processing, re-casting and step-by-step cooling of motor case materials. Compared with the prior art, the casting method capable of preventing deformation of the complex motor case has the following advantages that chromium carbide, zinc nitride and sulfur powder are added in the high temperature nitrogen protection atmosphere so that air entrapment can be avoided during melt casting, and excessive gas volume is avoided, the sand-type curing time can be prolonged, sand dropping or sand crushing in the casting process is avoided, and after columnar mold stripping, cooling is conducted first, then heating is conducted, the cooling speed is controlled, so that the problem of local shrinkage of the complex motor case can be avoided, the finish degree of the surface of a formed part is improved, and defects of blowholes, slag holes and sand holes are prevented; the product yield reaches 97%, wherein the problems of blowholes, sand holes and shrinkage accounts for about 25% of the scrap rate, and deformation of the complex motor case can be reduced effectively.

The invention discloses a modified polyethylene composite nanomaterial. The modified polyethylene composite nanomaterial is prepared from, by mass, 80-90 parts of carbon black modified polyethylene, 100-120 parts of nano-silicon carbide modified polyethylene, 100-120 parts of nano-zinc nitride modified polyethylene, 40-50 parts of titanium carbide modified polyethylene, 30-40 parts of nano-silver powder modified polyethylene, 10-15 parts of carbon fibers, 45-50 parts of teflon, 8-10 parts of chloroprene rubber, 10-12 parts of butadiene rubber, 13-15 parts of butadiene-acrylonitrile rubber, 4-5 parts of silicone rubber, 6-8 parts of polycarbonate, 5-6 parts of tetrabutyl titanate, 10-12 parts of titanium dioxide, 6-8 parts of iron boride and 5-6 parts of calcium silicide. The modified polyethylene composite nanomaterial is high in strength, excellent in heat resistance and flame retardance, good in heat stability and uniform in dispersion, the flame retardance, heat resistance, oil resistance and strength of the composite material are improved, and meanwhile the fluidity and processability of the composite material are improved.

The invention discloses a conductive ink composite material which is prepared from the following raw material formula components in parts by mass: 30-35 parts of polypyrrole, 5-6 parts of sodium borohydride, 45-50 parts of phenylenediamine, 6-8 parts of ferroferric oxide, 20-25 parts of zinc nitride composite nanometer silver powder, 20-30 parts of silicon nitride composite nanometer copper powder, 25-30 parts of silicon carbide composite nanometer silver powder, 8-10 parts of silicon carbide silicon carbide composite nanometer copper powder, 25-30 parts of titanium nitride composite nanometer zinc powder, 30-35 parts of titanium carbide composite nanometer silver powder, 14-20 parts of dimethylsilicone fluid and 10-15 parts of glycerin. The conductive ink composite material is reasonable in component configuration, high in adhesive force, excellent in conductivity, low in preparation cost and high in stability, and the dispersing stability of the conductive ink can be improved.