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Activated composite absorption air purifying agent and preparation method thereof

An air purifier and composite adsorption technology, applied in the field of air purification, can solve problems such as inability to purify organic gases, and achieve the effect of excellent surface catalytic activity and high specific surface area

Inactive Publication Date: 2018-12-18
WUHU SAUNAKING ELECTRONICS TECH CO LTD
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Ordinary air purification filter elements can only adsorb dust in the air, but cannot purify organic gases

Method used

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  • Activated composite absorption air purifying agent and preparation method thereof

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preparation example Construction

[0015] The present invention also provides a preparation method of the activated composite adsorption type air purifier, comprising the following steps:

[0016] (1) Mix organic silicate and organic titanate evenly to obtain mixed sol A, then add the zeolite-like imidazole skeleton material into mixed sol A, and ultrasonically disperse for 20 to 45 minutes to obtain mixed sol B, and then Add cetyltrimethylammonium bromide solution dropwise to the mixed sol B. After the dropwise addition, add a pH regulator to adjust the pH of the system to 5.3-6.2, and then seal the mixed system at 100-160°C for 1 ~4h, the product was washed and dried by centrifugation to obtain intermediate product 1;

[0017] (2) After polyepichlorohydrin dimethylamine is uniformly dispersed in water, intermediate product 1 is added, ultrasonically reacted for 15-25 minutes, and then centrifugally washed and dried to obtain intermediate product 2;

[0018] (3) Calcining the intermediate product 2 at 300-500...

Embodiment 1

[0024] An activated composite adsorption type air cleaner is made of the following parts by weight: 28 parts by weight of zeolite-like imidazole framework material (Zn-ZIF), 14 parts by weight of tetraethyl titanate, and 2 parts by weight of tetrabutyl silicate , 20 parts by weight of polyepichlorohydrin dimethylamine, 10 parts by weight of cetyltrimethylammonium bromide, 5 parts by weight of 2M hydrochloric acid, and 30 parts by weight of N,N-dimethylformamide.

[0025] The preparation method of the activated composite adsorption type air purifier, the steps are as follows:

[0026] (1) Dissolve zinc chloride and 2-methylimidazole in N, N-dimethylformamide (the molar ratio of zinc chloride and 2-methylimidazole is 1:8), pour the zinc chloride solution into the 2-methylimidazole solution, and stirred at 50°C for 12 hours, washed, centrifuged, and dried to obtain the zeolite-like imidazole framework material (Zn-ZIF);

[0027] Mix tetrabutyl silicate and tetraethyl titanate ev...

Embodiment 2

[0031] An activated composite adsorption type air cleaner is made of the following parts by weight: 20 parts by weight of zeolite-like imidazole framework material (Zn-ZIF), 5 parts by weight of tetraethyl titanate, and 1 part by weight of tetrabutyl silicate , 8 parts by weight of polyepichlorohydrin dimethylamine, 12 parts by weight of cetyltrimethylammonium bromide, 8 parts by weight of 2M hydrochloric acid, and 50 parts by weight of tetrahydrofuran.

[0032] The preparation method of the activated composite adsorption type air purifier, the steps are as follows:

[0033] (1) Dissolve zinc chloride and 2-methylimidazole in tetrahydrofuran (the molar ratio of zinc chloride and 2-methylimidazole is 1:10), and pour the zinc chloride solution into the 2-methylimidazole solution , and stirred at 45°C for 10 hours, washed, centrifuged, and dried to obtain the zeolite-like imidazole framework material;

[0034] Mix tetrabutyl silicate and tetraethyl titanate evenly to obtain mixe...

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Abstract

The invention relates to the technical field of automobile spare parts, in particular to an activated composite absorption air purifying agent and a preparation method thereof. The preparation methodcomprises the steps of: compounding organic silicate ester, organic titanate and the zeolite-like imidazole skeleton material to obtain an intermediate product 1; dispersing polyepichlorohydrin dimethylamine in water evenly, then adding the intermediate product 1, carrying out ultrasonic reaction for 15-25min, then performing centrifugal washing and drying to obtain an intermediate product 2; androasting the intermediate product 2 at 300-500DEG C for 2-6h, thus obtaining the activated composite absorption air purifying agent. The activated composite absorption air purifying agent provided bythe invention has excellent catalytic performance, can effectively adsorb pollutants in the air and achieve in situ degradation on pollutants, thus having broad application prospects in the air purification field.

Description

technical field [0001] The invention relates to the technical field of air purification, in particular to an activated composite adsorption air purifier and a preparation method thereof. Background technique [0002] The quality of indoor air is an important factor affecting human health and thoughts and emotions. When the concentration of VOCs (volatile organic compounds) in the indoor air is too high, it is easy to cause acute poisoning. In mild cases, headache, dizziness, cough, nausea, vomiting, or drunkenness will occur; in severe cases, liver poisoning and even coma will occur soon , and some may be life-threatening. Living in a room polluted by VOCs for a long time can cause chronic poisoning, damage the liver and nervous system, cause general weakness, drowsiness, and itchy skin. Some may also cause endocrine disorders and affect sexual function; benzene and xylene can also damage the system and even cause leukemia. At present, it has been identified as a carcinog...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D53/86B01D53/02B01J20/22B01J20/30
CPCB01D53/86B01D53/02B01D2255/20707B01D2255/802B01J20/226
Inventor 马西健崔亮
Owner WUHU SAUNAKING ELECTRONICS TECH CO LTD
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