The invention discloses a method for preparing polyepichlorohydrin-
dimethylamine-modified porous magnetic
glucan microspheres. The method is characterized by including the steps that mineral
ether,
dichloromethane and octacosane serve as organic phases;
glucan and nanometer Fe3O4 magnetic particles serve as water phases; the water phases are sprayed to the organic phases,
epoxy chloropropane is added, the mixture is frozen and dried for 24 h, and the porous magnetic
glucan microspheres are obtained; 64%-70% by
mass of
acetone, 2%-8% by
mass of ethanediamine and 8%-14% by
mass of
polyepichlorohydrin dimethylamine are added into a reactor and dissolved, 12%-20% by mass of the porous magnetic glucan microspheres are added, the sum of all the components are 100%, and all the components are stirred and subjected to a
reflux reaction for 4 h to 6 h at the constant temperature of 50 DEG C+ / -2 DEG C, cooling is carried out, then the product is washed with deionized water and
acetone, subjected to
solid-liquid separating and dried, and the polyepichlorohydrin-
dimethylamine-modified porous magnetic glucan microspheres are obtained; an adsorbent has the quite-high adsorption capacity for
bisphenol A and is repeatedly used, the cost is low,
environmental protection is achieved, and meanwhile
magnetism is easy to separate.