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Preparation method of organosilicone synthetic leather

An organosilicon synthetic leather and organosilicon technology, applied in the field of synthetic leather, can solve the problems of poor bonding fastness and easy generation of static electricity by organosilicon synthetic leather, and achieve tough film formation, excellent scratch resistance and good weather resistance. Effect

Active Publication Date: 2018-12-21
福建新隆上超纤有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Therefore, in view of the above content, the present invention provides a method for preparing organic silicon synthetic leather, which solves the problems of easy generation of static electricity and poor bonding fastness of existing organic silicon synthetic leather.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] (1) Preparation of surface glue

[0029] Mix 100 parts by weight of dimethyldichlorosilane monomer, 0.3 parts by weight of catalyst N,N-dimethylbenzylamine and 60 parts by weight of distilled water and stir evenly; then condense and reflux at 90°C in the reactor React for 10 hours to obtain an active silicone component; get 100 parts by weight of the active silicone component, 10 parts by weight of vinyltrimethoxysilane monomer, 0.3 parts by weight of catalyst N,N-lutidine, 60 parts by weight of distilled water are mixed and placed in a reaction kettle, condensed and refluxed at 120°C for 2 hours to obtain an organosilicon hybrid; 100 parts by weight of the organosilicon hybrid, 10 parts by weight of DM10, 5 parts by weight Inhibitor methyl butynol, 0.1 parts by weight photoinitiator, 0.5 parts by weight defoamer, 2 parts by weight antistatic agent JL-E26, 20 parts by weight solvent triethanolamine and 0.5 parts by weight catalyst zinc oxide; The agent is a mixture of ...

Embodiment 2

[0035] A preparation method of organic silicon synthetic leather, the steps are as follows:

[0036] (1) Preparation of surface glue

[0037] Mix 100 parts by weight of dimethyldichlorosilane monomer, 0.5 parts by weight of catalyst N,N-dimethylbenzylamine and 70 parts by weight of distilled water and stir evenly; then condense and reflux at 100°C in the reactor React for 9 hours to obtain an active silicone component; get 100 parts by weight of the active silicone component, 20 parts by weight of vinyltrimethoxysilane monomer, 0.5 parts by weight of catalyst N,N-lutidine, 70 parts by weight of distilled water are mixed and placed in a reaction kettle, condensed and refluxed at 130°C for 1 hour to prepare an organosilicon hybrid; 100 parts by weight of the organosilicon hybrid, 20 parts by weight DM10, 10 parts by weight Inhibitor methyl butynyl alcohol, 0.3 parts by weight of photoinitiator, 5 parts by weight of defoamer, 5 parts by weight of antistatic agent JL-E26, 60 part...

Embodiment 3

[0043] A preparation method of organic silicon synthetic leather, the steps are as follows:

[0044] (1) Preparation of surface glue

[0045] Mix 100 parts by weight of dimethyldichlorosilane monomer, 0.4 parts by weight of catalyst N,N-dimethylbenzylamine and 65 parts by weight of distilled water and stir evenly; then condense and reflux at 95°C in the reactor React for 9.5 hours to obtain an active silicone component; get 100 parts by weight of the active silicone component, 15 parts by weight of vinyltrimethoxysilane monomer, 0.4 parts by weight of catalyst N,N-lutidine, 65 parts by weight of distilled water are mixed and placed in a reaction kettle, condensed and refluxed at 125°C for 1.5 hours to obtain an organosilicon hybrid; 100 parts by weight of the organosilicon hybrid, 15 parts by weight DM10, 8 parts by weight Inhibitor methyl butynol, 0.2 parts by weight of photoinitiator, 2 parts by weight of defoamer, 3 parts by weight of antistatic agent JL-E26, 40 parts by w...

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PUM

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Abstract

The invention relates to the technical field of synthetic leather, and provides a preparation method of organosilicone synthetic leather. The method comprises the steps that 1, surface glue is prepared; 2, bottom glue is prepared; 3, release paper is evenly covered by the surface glue through a roller painter according to thickness of 0.1-0.5 mm to obtain a surface glue layer, drying is conducted,on a second roller painter, according to thickness of 0.1-0.2 mm, the surface glue layer is evenly covered by a bottom glue material, then the surface glue layer and a base cloth are subjected to lamination, drying is conducted, and through a winder, the release paper of a semi-finished product is separated, so that the organosilicone synthetic leather is obtained. By means of the preparation method of the organosilicone synthetic leather, the problems that existing organosilicone synthetic leather is prone to generate static electricity and has poor bonding fastness are solved.

Description

technical field [0001] The invention relates to the technical field of synthetic leather, in particular to a method for preparing organic silicon synthetic leather. Background technique [0002] Silicone synthetic leather is a composite material composed of textile (or synthetic leather) base material, primer glue, surface glue and surface coating layer, etc. bonded in sequence. Compared with the very popular and best-selling polyurethane synthetic leather in the market, silicone synthetic leather has not achieved substantial promotion. The fundamental reason is the excellent cost performance of polyurethane synthetic leather. However, polyurethane synthetic leather always has defects in toxicity, environmental protection, weather resistance and water resistance, while silicone materials have environmental protection, weather resistance and hydrophobic properties, so silicone synthetic leather has always been regarded as a potential value. substitute. Although silicone syn...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06N3/00D06N3/12
CPCD06N3/0059D06N3/0063D06N3/0077D06N3/0097D06N3/12D06N2209/046D06N2209/103D06N2209/1664D06N2211/28
Inventor 王鑫
Owner 福建新隆上超纤有限公司
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