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White opacified glaze for jun porcelain

An opacifying glaze and white technology, applied in the field of Jun porcelain production, can solve the problems of low utilization rate of fly ash, high production cost, high cost, etc., achieve enhanced opacification effect, good opacification effect of glaze surface, high The effect of ornamental value

Inactive Publication Date: 2018-12-28
周彩云
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The kiln changes mainly come from the formula of the glaze and the strict firing process. The glazes commonly used in Yuzhou mainly include feldspar, this medicine, black medicine, quartz, talc, calcite, plant ash, bone ash, etc., and the modern Jun kiln In order to improve the firing rate, chemical reagents such as copper oxide, zinc oxide, and tin oxide are generally added to the formula, resulting in high production costs of Jun porcelain. At present, zircon is usually added to the white opaque glaze in the production of Jun porcelain. , leading to higher costs; and with the continuous exploitation of local glaze raw materials, it is also facing an increasingly severe trend of resource shortage; therefore, it is necessary to find a new alternative raw material
[0004] Fly ash is the fine ash produced by the combustion of coal powder or coal gangue powder in the process of coal-fired heating and power generation. The annual output of my country is huge. At present, the utilization rate of fly ash in my country is not high, and fly ash Its chemical composition is mainly silicon dioxide and alumina, which are similar to the commonly used raw materials of Jun porcelain. In recent years, there have been preliminary studies on the application of fly ash to ceramics, but the use of fly ash to make white opaque glaze Research has rarely reported

Method used

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  • White opacified glaze for jun porcelain
  • White opacified glaze for jun porcelain

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A white opaque glaze for Jun porcelain, prepared from the following raw materials in parts by weight: 26-34 parts by weight of white feldspar, 8-10 parts of fly ash, 12-18 parts of frit, 14-18 parts of quartz, 10-14 parts of calcite, and bone meal 2-4, magnesite 4-6, fluorite 4-6.

[0019] The used white feldspar, quartz, and calcite of the present invention are all taken from the local area of ​​Yuzhou, and the fly ash is purchased from the local area (the chemical composition content of the used fly ash is SiO 2 43.9, Al 2 o 3 35.6, Fe 2 o 3 6.18, CaO 4.39, MgO 1.21, K 2 O 0.68, Na 2 O0.71), because fly ash contains a lot of incomplete combustion impurities and iron content, it is easy to cause glaze holes and black centers during firing, and it is easy to make the overall glaze surface yellowish brown or even black, but fly ash It is easy to generate fine air bubbles during firing, which can produce an opacifying effect; on the basis of this, on the one hand...

Embodiment 2

[0025] A white opaque glaze for Jun porcelain, prepared from the following raw materials in parts by weight: 30 parts by weight of white feldspar, 9 parts by fly ash, 15 parts by frit, 16 parts by quartz, 12 parts by calcite, 3 parts by weight of bone meal, 5 parts by weight of magnesite, and 5 parts by fluorite .

[0026] The preparation method of Jun porcelain white opaque glaze as mentioned above comprises the following steps:

[0027] (1) Mix raw materials, remove iron, ball mill, and filter to obtain glaze slurry;

[0028] (2) Apply glaze to the body after bisque firing;

[0029] (3) Firing at 1280°C; the specific firing process is as follows: first, the temperature of the glazed green body is raised to 950°C evenly in 4 hours in an oxidizing atmosphere; then the temperature is raised to 1200°C in 6.5 hours in a reducing atmosphere ℃; Finally, under neutral fire, the temperature was evenly raised to 1280 ℃ in 4 hours; naturally cooled.

[0030] The glaze color of the p...

Embodiment 3

[0032] A white opaque glaze for Jun porcelain, prepared from the following raw materials in parts by weight: 30 parts by weight of white feldspar, 9 parts by fly ash, 15 parts by frit, 16 parts by quartz, 12 parts by calcite, 3 parts by weight of bone meal, 5 parts by weight of magnesite, and 5 parts by fluorite .

[0033] The preparation method of Jun porcelain white opaque glaze as mentioned above comprises the following steps:

[0034] (1) Mix raw materials, remove iron, ball mill, and filter to obtain glaze slurry;

[0035] (2) Apply glaze to the body after bisque firing;

[0036] (3) Firing at 1290°C; the specific firing process is as follows: first, the temperature of the glazed green body is raised to 970°C in 4 hours in an oxidizing atmosphere; then in a reducing atmosphere, the temperature is evenly raised to 1220°C in 7 hours ; Finally, under a neutral fire, the temperature was evenly raised to 1290 ° C in 4 hours; natural cooling.

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Abstract

White opacified glaze for jun porcelain is prepared from raw materials in parts by weight as follows: 26-34 parts of white feldspar, 8-10 parts of fly ash, 12-18 parts of frit, 14-18 parts of quartz,10-14 parts of calcite, 2-4 parts of bone powder, 4-6 parts of magnesite and 4-6 parts of fluorite. The fly ash replaces part of feldspar to be used as a main solvent, then, magnesite and fluorite areadded to relieve yellowish-brown influence caused by fly ash and adverse firing influence caused by high impurities and high loss on ignition, the opacifying effect caused by micro bubbles easily produced by the fly ash can be enhanced, the fly ash can be successfully used for firing of the white opacified glaze, the glaze is slight yellow ivory white, the glaze surface has a good opacifying effect, and the white opacified glaze has higher ornamental value.

Description

technical field [0001] The invention belongs to the technical field of Jun porcelain production, and in particular relates to a white opacified glaze of Jun porcelain. Background technique [0002] Jun porcelain is a special product in Yuzhou City, my country, and is one of the five famous ancient Chinese porcelains. Its production is mainly based on the scientific configuration of blanks and glazes, and the change of flame atmosphere is controlled during the firing process. The same glaze color can be fired to produce mottled kiln-changing colors, which is known as "one color in the kiln, and many colors out of the kiln". [0003] The kiln changes mainly come from the formula of the glaze and the strict firing process. The glazes commonly used in Yuzhou mainly include feldspar, this medicine, black medicine, quartz, talc, calcite, plant ash, bone ash, etc., and the modern Jun kiln In order to improve the firing rate, chemical reagents such as copper oxide, zinc oxide, and t...

Claims

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Application Information

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IPC IPC(8): C03C8/14C03C8/04C04B41/86
CPCC03C8/14C03C8/04C03C2204/04C03C2205/02C04B41/5022C04B41/86C04B41/4539C04B41/0072
Inventor 周彩云
Owner 周彩云
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