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A kind of preparation method of fine grain high specific gravity tungsten alloy

A high specific gravity, tungsten alloy technology, applied in the direction of additive manufacturing, energy efficiency improvement, process efficiency improvement, etc., can solve the problems of increasing manufacturing cost and manufacturing difficulty, complex preparation process, complicated process, etc. Simple and efficient material utilization

Active Publication Date: 2020-08-11
MATERIAL INST OF CHINA ACADEMY OF ENG PHYSICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the preparation process of this ultrafine / nanocomposite powder is complicated, and the subsequent preparation of fine-grained high-density tungsten alloy still needs to go through the processes of mixing, charging, pressing, and sintering. The entire manufacturing cost and manufacturing difficulty

Method used

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  • A kind of preparation method of fine grain high specific gravity tungsten alloy
  • A kind of preparation method of fine grain high specific gravity tungsten alloy

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Embodiment

[0029] The purpose of this embodiment is to provide a method for preparing fine-grained high-density tungsten alloys with high material utilization, no need for molds, simple preparation process, short preparation cycle, and high degree of automation, such as figure 1 shown, including the following steps:

[0030] (1) Taking materials according to the ratio: take the raw materials according to the following parts by weight and mix them to obtain mixed powder: 80-95 parts of pure tungsten powder, 5-20 parts of pure metal binder phase powder; the average particle size of the pure tungsten powder is 5-20 parts 20 microns, and the shape of tungsten powder is spherical, spherical or polygonal, so as to make it different from the pure metal binder phase powder; the average particle size of the pure metal binder phase powder is 30-150 microns, and the pure The metal binder phase powder can be tungsten powder, any powder of nickel powder, iron powder, copper powder, cobalt powder, man...

example

[0036] Example: Using laser rapid prototyping technology to prepare thin-walled samples of fine-grained high-density tungsten-nickel-iron alloy.

[0037] This preparation process comprises the following steps:

[0038] (1) Sieve commercial tungsten powder, iron powder, and nickel powder to obtain tungsten powder, nickel powder, and iron powder with an average particle size of 10 microns, 30 microns, and 130 microns, respectively, wherein the tungsten powder is polygonal in shape, and the nickel powder And the shape of iron powder is spherical. Weigh the powder according to the weight ratio of tungsten: nickel: iron = 90:7:3, put the powder into the material tank of the three-dimensional mixer, add stainless steel springs to promote stirring during the mixing process, and the mixing time is 1.5 hours.

[0039] (2) The mixed powder is baked in a vacuum oven at 80°C for 2 hours and then loaded into the powder feeder barrel of the laser rapid prototyping system. High-purity argon...

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Abstract

The invention discloses a preparation method of a fine-grained high-specific-gravity tungsten alloy, which comprises the following steps: (1) taking materials according to the ratio: 80-95 parts of pure tungsten powder, 5-20 parts of pure metal bonding phase powder; (2) raw materials Treatment: Dry the mixed powder under vacuum conditions, and then put it into the barrel of the powder feeder of the laser rapid prototyping system for standby; (3) Device preparation: Use high-purity argon to replace the atmosphere in the forming chamber, and then use the circulation purification method Reduce the water and oxygen content in the forming chamber; establish a three-dimensional model of the fine-grained high-density tungsten alloy sample to be processed, and perform layered slicing and path planning; (4) Laser preparation and forming: start the laser rapid prototyping system, coaxial output laser and The powder, according to the set slice information and scanning path information, is melted and deposited on the shaped substrate layer by layer. The method uses powder-feeding laser rapid prototyping technology to prepare fine-grained high-density tungsten alloys, which is simple, fast and efficient, and the size of the prepared tungsten grains is almost the same as that of the original tungsten powder.

Description

technical field [0001] The invention relates to the technical field of alloy material preparation, in particular to a method for preparing fine-grained high-density tungsten alloy by laser rapid forming technology. Background technique [0002] High specific gravity tungsten alloy is a two-phase alloy composed of tungsten particles and a bonding phase. There is also a certain solid solubility in the phase. High specific gravity tungsten alloys have a wide range of applications in aerospace, weapons, automobiles, energy, medical and other defense and civilian industries. [0003] Traditional high specific gravity tungsten alloys are generally formed by liquid phase sintering of raw tungsten powder with an average particle size of 0.5-6 microns and nickel, iron, copper and other powders with an average particle size of 1-6 microns. However, in the liquid phase sintering process The tungsten grains are dissolved and separated in the bonding phase, so that the original tungste...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C27/04C22C1/04B22F3/105
CPCC22C1/045C22C27/04B22F10/00B22F10/80B22F10/34B22F10/25B22F10/36B22F10/32Y02P10/25
Inventor 乐国敏马诗雨刘学李晋锋王小英周昱昭王斗
Owner MATERIAL INST OF CHINA ACADEMY OF ENG PHYSICS
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