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A kind of plugging agent and its preparation method and application

A technology of plugging agent and plugging slurry, applied in the field of plugging agent, can solve the problems of poor cementing ability, low viscosity of cement plugging agent, loss of gel properties, etc. The effect of a wide temperature range

Active Publication Date: 2021-11-30
PETROCHINA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In view of the above-mentioned lost circulation problems, especially the malignant lost circulation problems in fracture-cavity developed formations, complex fractured formations with high steep structures, or low pressure-bearing formations with long open-hole sections, conventional bridging and polymer gel plugging agents and The special fast-hardening cement plugging agent cannot be effectively solved. The main reasons include: the bridging plugging agent relies on the physical accumulation of particles, fibers, and sheet-like materials to form a plugging layer, and its cementing ability with the rock wall of the formation is poor. The "breathing effect" of internal pressure fluctuations and the effects of temperature and fluid immersion in the well may lead to the breakage of the "blocking partition wall". In addition, the particle size distribution of the bridging material is difficult to match the size of the formation leakage channel; the polymer gel is under pressure. Low capacity and easy to degrade under high temperature, thus losing gel properties, so the leaky layer cannot be effectively sealed; cement plugging agent has low viscosity, it is difficult to stay in the leaky layer, the construction procedure is complicated and the risk is high

Method used

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  • A kind of plugging agent and its preparation method and application

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] 1. Preparation of curing agent

[0024] Mix blast furnace slag, gypsum, and aluminum silicate fibers in a mass ratio of 25:1:4, then dry and grind them. The drying temperature is 90°C and the drying time is 24 hours to obtain a curing agent.

[0025] 2. Preparation of filler

[0026] Calcium carbonate, asphalt, and nano-silicon powder are mixed according to the mass ratio of 6:2:2 to prepare the filler; among them, the particle size of calcium carbonate is 400 mesh; the particle size of asphalt is ≤40 mesh; the average particle size of nano-silicon powder The particle size is 30nm.

[0027] 3. Preparation of plugging agent

[0028] Mix sodium-based bentonite, the above-mentioned curing agent, alloy fiber, expansion agent, and the above-mentioned filler according to the mass ratio of 4:40:1:4:50 to prepare the plugging agent. Among them, the alloy fiber is polyethersulfone / polytetrafluoroethylene alloy fiber modified by silicon dioxide, activated calcium carbonate and...

Embodiment 2

[0032] 1. Preparation of curing agent

[0033] Mix blast furnace slag, gypsum, and silicate fiber in a mass ratio of 15:1:5, then dry and grind at a drying temperature of 90°C and a drying time of 24 hours to obtain a curing agent; among them, silicate The fiber is made by mixing aluminum silicate fiber and asbestos wool according to the mass ratio of 1:1.

[0034] 2. Preparation of filler

[0035] Calcium carbonate, asphalt, and nano-silicon powder are mixed in a mass ratio of 9:1:3 to obtain a filler; the particle size of calcium carbonate is 800 mesh; the particle size of asphalt is ≤40 mesh; the average particle size of nano-silicon powder The particle size is 50nm.

[0036] 3. Preparation of plugging agent

[0037] Mix the calcium-based bentonite, the above-mentioned curing agent, alloy fiber, expansion agent and the above-mentioned filler uniformly according to the mass ratio of 4:45:1:5:41 to prepare the plugging agent; wherein, the alloy fiber is made of silica, Ac...

Embodiment 3

[0041] 1. Preparation of curing agent

[0042] Mix blast furnace slag, gypsum, and silicate fiber in a mass ratio of 22:1:2, then dry and grind at a drying temperature of 90°C and a drying time of 24 hours to obtain a curing agent; among them, silicate The fiber is made of aluminum silicate fiber, sepiolite mineral fiber and asbestos wool in a mass ratio of 1:1:1.

[0043] 2. Preparation of filler

[0044] Calcium carbonate, asphalt, and nano-silicon powder are mixed in a mass ratio of 10:3:3 to obtain a filler; the particle size of calcium carbonate is 1250 mesh; the particle size of asphalt is ≤40 mesh; the average particle size of nano-silicon powder The particle size is 80nm.

[0045] 3. Preparation of plugging agent

[0046] Mix sodium-based bentonite, the above-mentioned curing agent, alloy fiber, expansion agent and the above-mentioned filler according to the mass ratio of 3:40:1:7:48 to prepare a plugging agent; wherein, the alloy fiber is made of silica, Activated...

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Abstract

The invention provides a plugging agent, a preparation method and application thereof. The plugging agent includes the following components by weight: 1-8 parts of bentonite, 10-50 parts of curing agent, 0.5-4 parts of alloy fiber, 2-8 parts of expansion agent and 20-50 parts of filler; wherein: bentonite is sodium One or both of base bentonite and calcium base bentonite; the curing agent is mixed with blast furnace slag, gypsum and silicate fiber according to the mass ratio (15‑30): (1‑2): (2‑6) It is dried and ground; the alloy fiber is polyethersulfone / polytetrafluoroethylene alloy fiber modified by silica, activated calcium carbonate and titanium dioxide; the expansion agent is granular silicone rubber and sheet silicone rubber One or two of them; the filler is mixed with calcium carbonate, asphalt and nano silicon powder in a mass ratio of (4‑12): (1‑3): (2‑6). The lost circulation agent is not restricted by the leakage channel, has a wide temperature range, and the solidified sealing layer has strong cementability with the wall surface of the leakage channel, which is convenient for popularization and application.

Description

technical field [0001] The invention relates to a leak-stopping agent, in particular to a leak-stopping agent and its preparation method and application. Background technique [0002] Lost circulation refers to the fact that various working fluids (including drilling fluid, cement slurry, completion fluid and other working fluids, etc.) enter the formation along the formation loss channel under the action of positive pressure difference during the drilling operation, and enter the larger liquid-holding reservoir in the formation. A downhole complex phenomenon of space. A series of downhole complex situations such as pipe sticking, blowout, and well collapse caused by lost circulation and the resulting vicious accidents have a great impact on drilling engineering. [0003] In view of the above-mentioned lost circulation problems, especially the malignant lost circulation problems in fracture-cavity developed formations, complex fractured formations with high steep structures...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B28/14C09K8/48
CPCC04B28/14C04B2111/00008C04B2111/00724C04B2201/50C09K8/426C09K8/48C09K2208/08C04B14/104C04B18/142C04B14/46C04B16/06C04B24/42C04B14/28C04B24/36C04B18/146
Inventor 陈军向朝纲段永贤刘翔李有伟李巍李炜舒小波
Owner PETROCHINA CO LTD
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