A method for ultra-refinement of martensitic structure of steel for die-casting mold

A die-casting mold and martensite technology, which is applied in heat treatment equipment, manufacturing tools, quenching agents, etc., can solve the problems of lack of in-depth consideration of quenched martensite strip refinement, limited improvement of thermal fatigue resistance of steel for die-casting molds, etc. , to achieve the effect of shortening the heat treatment cycle, reducing the heat treatment cost and improving the impact toughness

Active Publication Date: 2020-11-17
GUANGDONG HONGTAI NANTONG PRECISION TECH CO LTD +1
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Problems solved by technology

[0013] The ultra-refinement of the microstructure of the invention patent is only aimed at the control of carbide precipitation. It adopts the method of high-temperature homogenization combined with isothermal spheroidization to refine and spheroidize alloy carbides, and does not consider the fineness of quenched martensite lath. However, high-temperature homogenization will bring grains and subsequent coarser martensitic laths, so this technology is still limited in improving the thermal fatigue resistance of steel for die-casting molds

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  • A method for ultra-refinement of martensitic structure of steel for die-casting mold
  • A method for ultra-refinement of martensitic structure of steel for die-casting mold

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Embodiment 1

[0039] On the basis of the composition of AISI H13 steel, add 0.3wt% ~ 0.6wt% Nb (niobium), after smelting, casting, 1200 ~ 1300 ℃ high temperature diffusion annealing for 12 hours (homogenization) and after forging (forging thickness 180 ~ 240mm ), ultra-fine treatment (isothermal ultra-fine in the two-phase area, to realize the spheroidization of carbides: heat preservation at 1030°C for 15 hours, quench to room temperature, heat to 830°C and heat preservation for 3 hours, cool to 760°C, continue heat preservation for 6~ 8h / 100mm), and then perform the following martensitic superfine heat treatment:

[0040] (1) The first stage of quenching and cooling process: 1030-1050°C vacuum insulation heat treatment for 2-6 hours; gas quenching with 3-5bar nitrogen or inert gas to reduce the surface temperature of the mold steel module to 260-270°C, and Keep at this temperature for 120s, and the temperature difference between the core and the surface of the forging is controlled at 50-...

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Abstract

The invention relates to a martensite tissue ultra-refining method of steel for a die-casting die. The method comprises the steps that (1) an ultra-refined forging is subjected to vacuum heat treatment and heat preservation, then is subjected to gas quenching, so that the temperature of the surface of the forging is reduced to 255-275 DEG C, the forging is kept at the temperature for 105-130 s, and thus the temperature difference between the surface and the core part of the forging is controlled to be 50-80 DEG C; (2) heat preservation is carried out under the protection atmosphere condition of 360-400 DEG C; (3) heat preservation is carried out at the temperature of 550-600 DEG C, and then the forging is subjected to oil quenching to room temperature; and (4) 1-3 times of de-stress tempering treatments are carried out till the hardness meets the requirements. The method is simple, easy to operate, and is particularly suitable for large-specification die steel; and the heat treatment period is shortened, the impact toughness is improved by 12%-20% under the conventional die casting requirement hardness condition, the service life of the die-casting die can be prolonged, and the hardness requirement of the high-performance die-casting die steel for aluminum alloy automobile part die-casting is met.

Description

technical field [0001] The invention belongs to metal heat treatment technology, in particular to a heat treatment method for steel for die-casting molds, especially a method for ultra-refining the martensite structure of steel for die-casting molds. Background technique [0002] AISI H13 (4Cr5MoSiV1) is currently the most widely used type of hot work die steel, which can be used for die casting dies, hot stamping dies, hot forging dies and extrusion dies. The hardness of H13 steel is generally ≥ 50HRC; as a die-casting mold steel, the generally accepted hardness is 44-48HRC. [0003] Martensite (martensite) is a name for the structure of ferrous metal materials. It is a supersaturated solid solution of carbon in α-Fe, which is formed by rapid cooling (quenching) of austenite. Martensitic stainless steel is a class of stainless steel whose properties can be adjusted by heat treatment (quenching, tempering). When the austenite reaches the martensite transformation temperatu...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C21D1/78C21D1/74C21D1/773C21D1/613C21D1/18
CPCC21D1/18C21D1/613C21D1/74C21D1/773C21D1/785C21D2211/008
Inventor 陈晓平吴日铭张新强刘后尧彭卫平葛云鹏谢海波
Owner GUANGDONG HONGTAI NANTONG PRECISION TECH CO LTD
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