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A special device for multi-station long tube high-efficiency magnetron sputtering coating

A technology of magnetron sputtering coating and special device, which is applied in the field of high-efficiency preparation of metal film materials, can solve the problems of long coating time, low coating success rate, large target size, etc. performance, achieving continuous effects

Active Publication Date: 2021-01-05
INST OF METAL RESEARCH - CHINESE ACAD OF SCI +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the method of rotation can be used to coat the film, the diffraction of the plasma still occurs during the film coating, which will cause quality problems of the film material, such as loose surface, etc.
In addition, the coating of materials such as pipes often has long workpieces, and ordinary equipment cannot complete the coating of long workpieces; the flat target is used to complete the coating of long pipes, either because the target size is large and the cost is high, or the coating time is long and the efficiency is low. also low

Method used

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  • A special device for multi-station long tube high-efficiency magnetron sputtering coating
  • A special device for multi-station long tube high-efficiency magnetron sputtering coating
  • A special device for multi-station long tube high-efficiency magnetron sputtering coating

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0047] Install the 304 stainless steel target in the ring target magnetron sputtering long tube coating special device, put the 1.2m coated copper tube into the equipment at the loading and unloading end of the sliding assembly of the magnetic coupling transmission system, and then seal the loading and unloading end. Start the mechanical pump to evacuate the vacuum chamber. When the vacuum reaches 8.5Pa, start the molecular pump to evacuate the vacuum chamber. At the same time, start the heating system at the core of the pipe to heat the copper pipe. Before coating, the base of the pipe The temperature is 200°C, when the vacuum reaches 5.3*10 - 3 At Pa, fill the argon gas through the charging port, adjust the power supply parameters, the sputtering voltage reaches 450V, the sputtering current reaches 1.5A, and the time for sputtering 304 stainless steel film for copper tube is 1min. During the coating process, the copper tube is moved from one end of the sputtering device to ...

Embodiment 2

[0050] Install the metal chromium target in the ring target magnetron sputtering long tube coating special device, put the 1.2m coated copper tube into the equipment at the loading and unloading end of the sliding assembly of the magnetic coupling transmission system, and then seal the loading and unloading end. Start the mechanical pump to evacuate the vacuum chamber. When the vacuum reaches 8.0Pa, start the molecular pump to evacuate the vacuum chamber. At the same time, start the heating system at the core of the pipe to heat the copper pipe. Before coating, the base of the pipe The temperature is 250°C, when the vacuum reaches 6.6*10 -3 At Pa, fill the argon gas through the charging end, adjust the power supply parameters, the sputtering voltage reaches 480V, the sputtering current reaches 1.8A, and the time for sputtering metal chromium film on copper tube is 3min. During the coating process, the copper tube is moved from one end of the sputtering device to the other end ...

Embodiment 3

[0053] Install the FeCrAl alloy target in the ring target magnetron sputtering long tube coating special device, put the 1.2m coated copper tube into the equipment at the loading and unloading end of the sliding assembly of the magnetic coupling transmission system, and then seal the loading and unloading end. Start the mechanical pump to evacuate the vacuum chamber. When the vacuum reaches 7.6Pa, start the molecular pump to evacuate the vacuum chamber. At the same time, start the heating system at the core of the pipe to heat the copper pipe. Before coating, the base of the pipe The temperature is 220°C, when the vacuum reaches 5.8*10 - 3 Pa, fill the argon gas through the gas filling port, adjust the power supply parameters, the sputtering voltage reaches 460V, the sputtering current reaches 1.6A, and the time for sputtering the FeCrAl alloy film for the copper tube is 1.5min. During the coating process, the copper tube is moved from one end of the sputtering device to the ...

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Abstract

The invention aims to provide a device special for efficient magnetron sputtering preparation of a high-quality metal film on the outer surface of a long pipe. A vacuum chamber communicates with a vacuum generating system and an inflation system, and the vacuum chamber is internally provided with an annular target sputtering system and a re-sputter cleaning system; a servo transmission system is connected with a magnetic coupling transmission system; the magnetic coupling transmission system is provided with an external magnetic ring, a front blocking pipe, a rear blocking pipe, a supporting pipe and a supporting rod, the supporting pipe sleeves the supporting rod, the front blocking pipe and the rear blocking pipe sleeve the supporting pipe, the rear blocking pipe and the supporting pipeare fixed together, the rear blocking pipe and an N pole of the external magnetic ring are fixed together, an S pole magnet is arranged outside the N pole of the external magnetic ring, and the position between the front blocking pipe and the rear blocking pipe is used for fixing the film-coated pipe; the supporting rod penetrates through the vacuum chamber, and a pipe core heating system is arranged on the position, at a film-coated pipe inlet of the vacuum chamber, of the supporting rod; and a power supply system is connected with the vacuum generating system, the inflation system, the annular target sputtering system, the servo transmission system, the pipe core heating system, the re-sputter system and a circulating water cooling system.

Description

technical field [0001] The invention relates to magnetron sputtering coating, and provides a device for efficiently preparing metal films on ultra-long pipes. Background technique [0002] In the society with the rapid development of science and economy, thin film materials, as a kind of functional materials, have received more and more attention. As a form of material, functional film has special properties in light, electricity, magnetism, heat, anti-corrosion, decoration, etc., so it is applied in related fields. Functional thin film materials are divided into: superconducting thin film, conductive thin film, resistive thin film, semiconductor thin film, insulating thin film, passivation and protective thin film, piezoelectric thin film, ferroelectric thin film, photoelectric thin film, magnetoelectric thin film, magneto-optical thin film, etc. . At present, the means of preparing thin films are mainly divided into two categories: physical vapor deposition and chemical ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C14/56C23C14/02C23C14/35
CPCC23C14/022C23C14/35C23C14/562
Inventor 刘实王晓光王永利熊良银李静崔勇李依依
Owner INST OF METAL RESEARCH - CHINESE ACAD OF SCI
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