Method for measuring prothioconazole residue in food
A technology of prothioconazole and a determination method is applied in the field of determination of prothioconazole residues in food, and achieves the effects of high sensitivity, easy operation and reduced matrix interference
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[0051] Example
[0052] Instruments and reagents used in this embodiment:
[0053] T18Basic homogenizer (IKA, Germany); CR21GⅢ high-speed refrigerated centrifuge (Hitachi, Japan); MS3 vortex mixer (IKA, Germany); 1200 high performance liquid chromatography-UV detector (Agilent, USA); PSA dispersion Solid phase extraction agent (Agilent, USA); C18 dispersive solid phase extraction agent (Agilent, USA);
[0054] Reagents: water (ultra pure water, wah haha); acetonitrile (HPLC grade, Merke, Germany); ammonium formate (HPLC grade, CNW, Germany); formic acid (HPLC grade, CNW, Germany); ethyl benzoate (analytical pure , As an internal standard);
[0055] Prothioconazole standard substance: Purity 99.0%, purchased from Dr-Ehrenstorfer, Germany.
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