Preparing method of antibacterial anti-mite fabric
A fabric and anti-mite technology, applied in textiles and papermaking, fiber treatment, physical treatment, etc., can solve the problems of weakened anti-mite function of fabrics, easy shedding of anti-mite agents, and difficulty in lasting, so as to prolong the anti-mite effect and not easily run off. , the effect of inhibiting growth
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Embodiment 1
[0031] The bentonite modified by the quaternary ammonium salt used in embodiment 1, its modification method is:
[0032] a. Pulverize, dry and grind the raw bentonite, and then pass through a 400-mesh sieve;
[0033] b. Mix the sieved bentonite with 40% octadecyltrimethylammonium chloride solution, place it in a microwave heater and heat it for 4min, the microwave power is 600W, and the bentonite and octadecyltrimethylammonium The mass ratio of ammonium chloride is 1:4, and the pH of octadecyltrimethylammonium chloride solution is controlled to be 9;
[0034] c. After heating, filter the product with suction, wash once with sodium hydroxide solution with a pH of 9, wash twice with distilled water, freeze-dry the filter cake, activate it at 250°C for 1 hour, and grind it through a 400-mesh sieve. Obtain octadecyltrimethylammonium chloride modified bentonite.
Embodiment 2
[0035] The modification method of embodiment 2 and embodiment 3 is the same as embodiment 1, and the difference is that what embodiment 2 and embodiment 3 use is cetyltrimethylammonium chloride.
[0036] Example 1:
[0037] (1) Prepare ethanol and butanol with a volume ratio of 3:1 into an aqueous solution with a volume fraction of 40%, soak the linen fabric to be treated in the prepared aqueous solution of ethanol and butanol for 30min, and then use oxygen plasma Body treatment, wherein the oxygen plasma treatment conditions are: treatment time 6min, power 100W, pressure 25Pa;
[0038] (2) Soak the pure cotton fabric treated in step (1) with aminopropyltriethoxysilane solution, wherein the solution concentration is 3g / L, and aminopropyltriethoxysilane is 2.4% of the pure cotton fabric quality , the soaking time is 10min, after the end, put the fabric (with a liquid rate of 45%) in an oven at 50°C, and pre-dry for 30min;
[0039] (3) Dip the pre-dried fabric into anti-mite f...
Embodiment 3
[0047] (1) Prepare ethanol and butanol with a volume ratio of 4:1 into an aqueous solution with a volume fraction of 50%, soak the pure cotton fabric to be treated in the prepared aqueous solution of ethanol and butanol for 40min, and then use oxygen Plasma treatment, wherein the conditions of oxygen plasma treatment are: treatment time 7min, power 150W, pressure 35Pa;
[0048] (2) Soak the pure cotton fabric treated in step (1) with aminopropyltriethoxysilane solution, wherein the solution concentration is 4g / L, and aminopropyltriethoxysilane is 2.7% of the pure cotton fabric quality , soaking time 13min, after the end, put the fabric (with liquid rate 45%) in the oven at 45 ℃, pre-baked for 40min;
[0049] (3) Dip the pre-dried fabric into anti-mite finishing solution (evenly dispersed by ultrasonic) for padding, the bath ratio is 1:30, wherein the anti-mite finishing solution includes polyurethane adhesive, nano-silver and quaternary ammonium salt modification The concentr...
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