Multilayer-coated soft magnetic composite material and preparation method thereof
A soft magnetic composite material and multi-layer coating technology, which is applied in the direction of inorganic material magnetism, inductance/transformer/magnet manufacturing, electrical components, etc., can solve the problems of reducing the magnetic properties of composite materials and large eddy current losses, and achieve the improvement of heat treatment temperature , The effect of low eddy current loss
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Embodiment 1
[0060] A method for preparing a multilayer coated soft magnetic composite material, comprising the following steps:
[0061] (1) take by weighing the Fe powder of 50g, put into beaker;
[0062] (2) Measure 0.7ml of phosphoric acid and 99.3ml of alcohol respectively, and slowly add the passivating agent into the alcohol to make a passivating solution of 0.012g / ml;
[0063] (3) Measure 15ml of the phosphoric acid passivation solution, add it into a beaker, put it into a constant temperature water bath at 65°C, stir until the solution is completely evaporated to dryness, and obtain powder A;
[0064] The Al 2 o 3 The preparation of colloid comprises the steps:
[0065] (4) Take by weighing 4.0048g aluminum isopropoxide (grinding), put into beaker A after weighing;
[0066] (5) Measure 50ml of ethylene glycol ether in a graduated cylinder, add it to beaker A, and stir magnetically at 60°C for 30 minutes;
[0067] (6) Weigh 2.0024g of acetylacetone, slowly add it into beaker A...
Embodiment 2
[0079] A method for preparing a multilayer coated soft magnetic composite material, comprising the following steps:
[0080] (1) take by weighing the Fe powder of 50g, put into beaker;
[0081] (2) Measure 0.7ml of nitric acid and 99.3ml of alcohol respectively, and slowly add the passivating agent into the alcohol to make a passivating solution of 0.012g / ml;
[0082] (3) Measure 15ml of nitric acid passivation solution, add it into a beaker, put it into a constant temperature water bath at 65°C, stir until the solution is completely evaporated to dryness, and obtain powder A;
[0083] The Al 2 o 3 The preparation of colloid comprises the steps:
[0084] (4) Take by weighing 4.0048g aluminum isopropoxide (grinding), put into beaker A after weighing;
[0085] (5) Measure 50ml of ethylene glycol ether in a graduated cylinder, add it to beaker A, and stir magnetically at 60°C for 30 minutes;
[0086] (6) Weigh 2.0024g of acetylacetone, slowly add it into beaker A, and stir m...
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