The application relates to the technical field of inorganic functional material preparation, and is a production process of low-magnetic
nickel protoxide, which comprises the following steps: pretreatment of a
nickel chloride solution: pretreating
nickel chloride hexahydrate to obtain pretreated nickel
chloride solution; preparation of coarse
nickel protoxide: pumping the pretreated nickel chloride solution into a centrifugal atomizer of a
spray pyrolysis device to form fine mist droplets, the mist droplets entering a
pyrolysis furnace along with
compressed air, three temperature zones being arranged in the
pyrolysis furnace, and the coarse
nickel protoxide being prepared by precisely controlling temperature and gas amount; and preparation of a low-magnetic
nickel oxide product; the application takes the nickel chloride solution as
raw material, controls the pretreatment complexing agent, optimizes
spray pyrolysis atomization parameters and carries out low-temperature ball milling dispersion, so that the magnetic property is reduced, the particles are uniformly dispersed and there is no obvious agglomeration phenomenon, the low-magnetic, small-particle-size
nickel protoxide product is prepared, and the problems of high product magnetic property,
large particle size and serious agglomeration in the preparation of the nickel protoxide by taking the nickel chloride solution as
raw material in the prior art are solved.