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150results about How to "High cost of preparation" patented technology

Preparation method of superfine nanometer lithium iron phosphate electrode material and application thereof

The invention discloses a preparation method of a superfine nanometer lithium iron phosphate electrode material, comprising the following steps of: firstly, taking an iron source compound and a phosphorus source compound as raw materials to obtain nanometer ferrous phosphate as a precursor; and secondly, using the ferrous phosphate and the lithium source compound to prepare the superfine nano lithium iron phosphate electrode material. The preparation method of ferrous phosphate, disclosed by the invention, has a simple production process; the obtained nanometer ferrous phosphate can be used for preparing the high-purity superfine nanometer lithium iron phosphate; and the ferrous valence state is not changed when the ferrous phosphate is used for preparing the lithium iron phosphate, thus, no carbon source compound or reducing agent needs to to be added to change the iron valence state, and then the carbon-coated lithium iron phosphate or non-carbon-coated lithium iron phosphate can be directly prepared. The nanometer lithium iron phosphate manufactured by the nanometer ferrous phosphate precursor has excellent performance, good discharge capacity and voltage platform performance under high capability and high multiplying power, and long cycle life.
Owner:GUANGXI NUOFANG ENERGY STORAGE TECH

Preparation method for core-shell fluorinated polyurethane-acrylate latex

The invention relates to a preparation method for core-shell fluorinated polyurethane-acrylate latex. The method comprises the following steps: placing polyether glycol and toluene diisocynate into a stirrer to prepare polyurethane; and emulsifying an emulsifier, butyl acrylate, methyl methacrylate, a functional monomer and a proper amount of water at high speed to prepare the core-shell fluorinated polyurethane-acrylate latex. By the method, the defects that the fluorinated acrylate in the prior art is independent of oil and water phases due to hydrophobicity and lipophobicity, effective micelle is difficult to form by the general surfactant and the grafting ratio is low are overcome. The core-shell fluorinated polyurethane-acrylate latex has a core-shell structure and the fluorinated acrylate is enriched in the shell, so a latex film has a large water contact angle. The using amount of the fluorinated acrylate monomer (G04) is 1 to 2 percent of the weight of the monomer and the using amount of polyurethane (PU) is 10 percent of the weight of a composite latex solid, so the preparation cost is low. The emulsifier does not need a fluorine-containing surfactant, so the polymerization rate is high, the grafting efficiency of the fluorinated acrylate monomer is high and the latex is stored stably.
Owner:江苏日出化工有限公司 +1

Preparation method of porous perfluorinated sulfonic acid resin for catalysts

The invention relates to a preparation method of porous perfluorinated sulfonic acid resin for catalysts, wherein the preparation method comprises that perfluoro(sulfonyl vinyl)ether and tetrafluoroethylene are polymerized under the condition of co-existence of a solvent, a pore-forming agent and an initiating agent to obtain the product, the perfluorinated sulfonic acid resin having low equivalent weight and low molecular weight is used as the pore-forming agent, the solvent is recycled by a way of adding deionized water and a dispersant and carrying out distillation, at the same time, the resin is molded, after further drying, a granular material is obtained, and moreover, a mixture of one or more of perfluorinated hydrocarbon / perfluorinated cyclic ether / chlorofluorocarbon are used as an extraction agent for extracting the pore-forming agent so as to form a porous structure. The method has simple operating conditions, has no need for high temperature and high pressure, and solves the problem in the prior art that effective catalytic component loss is difficult to overcome during a using process, and the service life of the catalyst is increased; and at the same time, due to the existence of the porous structure, the specific surface area is increased, and the active component utilization rate is improved.
Owner:SHANDONG DONGYUE WEILAI HYDROGEN ENERGY MATERIAL CO LTD

Thin film crystalline silicon perovskite heterojunction solar battery and preparation method thereof

ActiveCN105226187AOvercome the disadvantage of low light absorption coefficientReduce compoundingSolid-state devicesSemiconductor/solid-state device manufacturingHeterojunctionHole transport layer
The invention relates to a thin film crystalline silicon perovskite heterojunction solar battery and a preparation method thereof, and relates to a semiconductor device for converting luminous energy into electric energy. The thin film crystalline silicon perovskite heterojunction solar battery includes a transparent conductive substrate, a P-type thin film crystalline silicon hole transport layer, a perovskite light absorption layer, an electron transport layer formed by compact titanium dioxide, and a back electrode, wherein the perovskite light absorption layer and the P-type thin film crystalline silicon hole transport layer have matched energy levels. The configuration pattern: the P-type thin film crystalline silicon hole transport layer is arranged on the transparent conductive substrate; the perovskite light absorption layer is arranged on the P-type thin film crystalline silicon hole transport layer; the perovskite light absorption layer and the P-type thin film crystalline silicon hole transport layer form a thin film crystalline silicon perovskite heterojunction; the electron transport layer formed by the compact titanium dioxide is arranged on the perovskite light absorption layer; the back electrode is arranged on the electron transport layer formed by the compact titanium dioxide. According to the invention, the defects that the existing perovskite solar battery is low in stability and high in preparation cost, and a mass of silicon materials are used can be overcame.
Owner:HEBEI UNIV OF TECH

Combination switchable glass composite window and preparation method thereof

ActiveCN107526226AImprove featuresImprove uniformity and longevityCoatingsNon-linear opticsLaminated glassToughened glass
The invention relates to a combination switchable glass composite window and a preparation method thereof. The composite window and the preparation method thereof include a substrate, and a first outer ITO transparent conductive film layer, an electrochromic layer, an ion transport layer, an ion storage layer and a second outer ITO transparent conductive film layer which are sequentially arranged on the outer surface of the substrate, and further include an inner ITO transparent conductive film layer, a PDLC liquid crystal light-adjusting film and an ITO transparent conductive film which are sequentially arranged on the inner surface of the substrate, wherein ordinary glass, toughened glass, laminated glass, organic glass or a mixture thereof is selected and used for the substrate, tungsten oxide is selected and used for thin-film material of the electrochromic layer, a lithium ion thin film is selected and used for an ionic conductive layer, and nickel oxide thin film is selected and used for the ion storage layer. The composite window and the preparation method thereof have the advantages that a combination of the electrochromic layer and the PDLC liquid crystal light-adjusting film combines the advantages and disadvantages of both and further effects of intelligent light adjusting and light shielding can be achieved.
Owner:JIANGSU FANHUA GLASS CO LTD

Seedling medium and preparation method thereof

The invention relates to a seedling medium and a preparation method thereof, wherein the medium comprises the following components of raw materials: one or more of crop by-products, organic wastes, by-products generated in grass pulping process when preparing materials, and ammonia water. The method comprises the following steps: mixing one or more of the crop by-products, the organic wastes, theby-products of the grass pulping process when preparing the materials, and the ammonia water, and then fermenting to gain the medium, wherein nitrogenous condensate water generated when concentratingblack liquid generated in a neutral ammonium sulfite process is optimally selected as the ammonia water, and optimally, the condensate water with 0.05-0.55% of nitrogen content and at the temperatureof 25-70 DEG C is the best; and by-products generated in preparation department in the neutral ammonium sulfite process are optimally selected as the crop by-products. The method re-uses the waste and waste liquid which are generated in the neutral ammonium sulfite process to turn waste into wealth. The permeability and nutrient content of the medium are respectively superior to that of peat perlite, when the medium is used in the growth test of nursery stock of forest, the nursery stock has obvious grow, and the quantity of the root system can be increased by over 30 percent.
Owner:SHANDONG TRALIN PAPER

High-quality harmless utilizing method of hyperaccumulator

The invention discloses a high-quality harmless utilizing method of a hyperaccumulator. The high-quality harmless utilizing method comprises the following steps: smashing and drying the hyperaccumulator, and sieving through a sieve of which the density is 100 meshes; carbonizing at a carbonization temperature being 450 to 550 DEG C and in carbonization time being 25 to 35 minutes, thus obtaining acarbonized material; immersing the carbonized material by using an alkaline solution of which the mass percentage is 45 to 55 percent; drying at 90 to 120 DEG C for 10 to 15 hours after immersing for20 to 28 hours, thus obtaining an amorphous particulate carbon block; activating the amorphous particulate carbon block into an activated carbon coarse product under a nitrogen atmosphere, wherein the activating temperature is 750 to 850 DEG C, and the activation time is 25 to 35 minutes; drying for 10 to 15 hours, thus obtaining metal-containing activated carbon with a catalytic effect; grindingthe activated carbon, thus obtaining an activated product HA-AC; adding 5 to 15 percent of the activated carbon product HA-AC to biomass or other reaction raw materials; putting a swelled material ina supercritical reaction kettle, and carrying out sealing reaction at the reaction temperature being 380 to 600 DEG C and the reaction pressure being 22.1 to 30 MPa, thus obtaining a hydrogen-rich gas. The high-quality harmless utilizing method disclosed by the invention has the advantages that additional metal loading is not required, a complicated preparation technology and a longer preparationperiod are not required, heavy metal can be fully stabilized, and secondary pollution can be avoided.
Owner:NINGBO INST OF TECH ZHEJIANG UNIV ZHEJIANG

High ultraviolet transmitting double-layer wire grid polarizer for fabricating photo-alignment layer and fabrication method thereof

The present invention relates to a high ultraviolet transmitting double wire grid polarizer for fabricating a photo-alignment layer and a fabrication method thereof for improving the fabrication efficiency of the photo-alignment layer. More specifically, the invention provides a high ultraviolet transmitting double wire grid polarizer comprising: a substrate; a reflection preventing layer which is formed on the substrate; a patterned photosensitive material layer which is formed on the reflection preventing layer; and double metal thin film layers which are respectively formed on the photosensitive material layer and the reflection preventing layer. Further, the invention provides a fabrication method of a high ultraviolet transmitting double wire grid polarizer, the method comprises the steps of: forming a reflection preventing layer on a substrate; forming a photo sensitive material layer by applying photoresist to the top of the reflection preventing layer; forming a wire grid pattern by developing the photosensitive material layer after selectively exposing the photosensitive material layer according to a pattern that is formed by the laser interference light; and depositing metal on the wire grid pattern. Thus, the invention smoothly forms a wire grid by using the reflection preventing layer when the double wire grid polarizer is fabricated, and cuts down the production cost with no need to perform a dry etching process since the metal is deposited after the wire grid of the photosensitive material layer is formed. Further, compared with the existing single wire grid polarizer, the invention improves transmittance and polarization of the ultraviolet region, thereby enhancing the efficiency of the fabrication process of the photo-alignment layer.
Owner:LG CHEM LTD

Method for lithium extraction through extraction-reverse extraction, separation and purification

The invention relates to a method for lithium extraction through extraction-reverse extraction, separation and purification. The method comprises the following steps: (1) an extracting system containing a composite extracting agent is adopted to extract and separate lithium-contained solution under a condition of pH=10-13 to obtain a lithium-loaded organic phase; (2) the gas-liquid-liquid three-phase reverse extraction is performed on the lithium-loaded organic phase obtained in the step (1) to obtain lithium-loaded reverse extracting liquid; and (3) the reverse extracting liquid obtained in the step (2) is heated and separated to obtain a lithium product and separated mother liquor. The method realizes efficient separation of lithium from such impurity elements as Na, K and B by adoptingthe composite extracting agent, adopts the gas-liquid-liquid three-phase continuous reverse extraction to reach the reverse extracting rate of lithium is 90% above, the total yield is 83% or above andthe purity of the lithium product is 96% above, is high in treatment quantity, simple in process and equipment and low in investment, effectively utilizes industrial tail gas, and achieves energy conservation, environmental protection and continuous production.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI +1

Graphene and carbon nano tube enhanced aluminum matrix composite and preparation method thereof

ActiveCN110331318ATroubleshoot enhancementsOvercoming the problem of partial interface responseLiquid/solution decomposition chemical coatingCopper platingCarbon nanotube
The invention relates to a graphene and carbon nano tube enhanced aluminum matrix composite and a preparation method thereof, and belongs to the technical field of aluminum matrix composites. In orderto solve the problems that graphene and carbon nano tubes are clustered and form carbide with an aluminum matrix at a high temperature and in order to improve the wear resistance of the aluminum matrix composite, the graphene and carbon nano tube enhanced aluminum matrix composite is provided, and components of the graphene and carbon nano tube enhanced aluminum matrix composite comprise, by masspercent, 0.1%-5.0% of composite copper plated nickel graphene, 0.1%-5.0% of composite copper plated nickel carbon nano tubes, 5% of magnesium powder and the balance aluminum powder. Copper plated nickel is compounded on the surfaces of the graphene and the carbon nano tubes to strictly control the interface reaction, ultrasonic dispersion is carried out in a stirring state so that the graphene and the carbon nano tubes can be evenly dispersed in the aluminum matrix composite, finally the enhanced aluminum matrix composite is obtained through vacuum hot-pressing sintering, and the wear resistance of the aluminum matrix composite is obviously improved due to the self-lubricating characteristic of the graphene and the carbon nano tubes.
Owner:HEILONGJIANG UNIVERSITY OF SCIENCE AND TECHNOLOGY

Electrolytic and nitrogen-doping one-step method for preparing petroleum coke-based carbon quantum dots

The invention belongs to the scientific field of carbon nano-materials and relates to an electrochemical method for preparing petroleum coke-based carbon quantum dots and doping nitrogen in a one-step manner. In the invention, petroleum coke, which has high carbon content, low ash and a developed graphite lamellar structure, is creatively selected as a carbon source, and through an electrochemical oxidizing method, a novel technical method of preparing the carbon quantum dots is developed. Through change on calcination temperature, types of electrolytes and current density, fluorescent performance of the carbon quantum dots can be regulated. By means of addition of a nitrogen-doping agent to the electrolyte, preparation of nitrogen-doped carbon quantum dots through the electrochemical method in one step is achieved, and for the first time, ethylenediamine is employed as the electrolytic nitrogen-doping agent. Meanwhile, for the first time, foam nickel is creatively employed instead of a conventional Pt electrode, so that the method greatly increases electrolytic efficiency and reduces preparation cost. The petroleum coke is easy to obtain and low in cost. The whole process is simple in operation process, is convenient to product the carbon quantum dots industrially in large scale. The carbon quantum dots have wide application prospects in the fields of photo-catalysis, bio-imaging, and detection of ions and macromolecules.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Preparation method for blending modification of ultrafiltration membrane by using nano cellulose crystal

The invention discloses a preparation method for blending modification of an ultrafiltration membrane by using nano cellulose crystal, belonging to the field of preparation of membrane materials. Thepreparation method solves the problems that the nano material is expensive in the process of blending modification of ultrafiltration membrane by the existing nano material, and the material dispersibility is not good, the hydrophilicity is insufficient and the material is inclined to agglomerate in the preparation process. The preparation method firstly ultrasonically disperses the nanocellulosecrystals in an organic solvent, then adds the additive and the polymer film material, heats and stirs uniformly, and performs vacuum defoaming to obtain a casting liquid; the casting liquid is evenlyscraped onto the non-woven fabric, and the modified ultrafiltration membrane is obtained by undergoing a coagulation bath. The preparation method makes good use of the hydrophilicity and mechanical strength of the nanocellulose crystal, greatly improves the anti-pollution performance, the water flux and the mechanical strength of the ultrafiltration membrane, and prolongs the service life of the membrane. Simultaneously, the modified nano materials derive from a wealth of sources, and are cheap and easy to obtain, and have good dispersibility in the solvent, so that the ultrafiltration membrane is relatively low in cost and convenient for industrial production.
Owner:HAINAN LITREE PURIFYING TECH CO LTD
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