Environment-friendly spirodiclofen diester nano powder and preparation method thereof
An environmentally friendly, spirodiclofenac technology, applied in the field of pesticides, can solve the problems of poor quick-acting, narrow control surface, high cost, and achieve the effect of large surface area and high efficacy
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Embodiment 1
[0024] An environment-friendly spirodiclofen nano-powder, comprising active ingredient A, the active ingredient A is spirobudiglycol, 27wt% active ingredient, 12wt% solvent, 10wt% small molecule auxiliary agent, polymer auxiliary agent 5wt%, dispersant water 46wt%.
[0025] Wherein, solvent selects acetone for use.
[0026] Among them, the small molecule additives are selected from biodegradable small molecule additives, including anionic surfactants or nonionic surfactants, and ionic surfactants include carboxylate salts of linear alkyl groups with different carbon numbers. , Sulfonate, non-ionic surfactants include polyoxyethylene ethers of linear alkyl ethers, esters, and amides with different carbon numbers. The HLB value of small molecule additives is 12-15, and the dosage is 10%.
[0027] Among them, water-soluble polymer additives are selected as polymer additives, including natural water-soluble polymers and their derivatives, and natural water-soluble polymers and th...
Embodiment 2
[0035] An environment-friendly spirodiclofen nano-powder, comprising active ingredient A, the active ingredient A is spirobudiclofen, the mass fraction of the active ingredient is 9wt%, and also includes 21wt% of solvent, 25wt% of small molecule auxiliary agent, 14wt% polymer additives and 31wt% dispersant water.
[0036] Wherein, solvent selects cyclohexanone for use.
[0037] Among them, the small molecule additives are biodegradable small molecule additives, including anionic surfactants, and ionic surfactants include carboxylates, sulfonates, and sulfates of linear alkyl groups with different carbon numbers. , the HLB value of small molecule additives is 12-15, and the dosage is 25%.
[0038] Among them, the polymer additives are water-soluble polymer additives, including natural water-soluble polymers and their derivatives. Natural water-soluble polymers and their derivatives include carboxymethyl chitosan, modified guar gum, tea soap white.
[0039] The preparation me...
Embodiment 3
[0046] An environment-friendly spirodiclofen nano-powder, including active ingredient A, the active ingredient A is spirobudiester, the active ingredient accounts for 10wt%, and also includes 18wt% of solvent, 20wt% of small molecule auxiliary agent, polymer auxiliary agent Agent 12wt% and dispersant water 40wt%.
[0047] Wherein, the solvent is selected from acetone and cyclohexanone mixed according to the volume ratio of 1:1.
[0048] Among them, the small molecule additives are biodegradable small molecule additives, including non-ionic surfactants, which include polyoxyethylene polyoxyethylenes composed of straight-chain alkyl ethers, esters, and amides with different carbon numbers. Ether, the HLB value of the small molecule additive is 12-15, and the dosage is 10-25%.
[0049]Among them, the polymer additives are water-soluble polymer additives, including synthetic polymers, and the synthetic polymers are selected from polyvinyl alcohol, sodium polyacrylate, polyacrylam...
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