Efficient environment-friendly acidic color fixing agent and preparation method thereof
An acid color fixing agent and environmental protection technology, applied in the field of printing and dyeing auxiliaries, can solve the problems of failing to meet environmental protection requirements, and achieve the effects of improving dry rubbing fastness, high degree of bonding, and broad application prospects.
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Embodiment 1
[0023] A high-efficiency and environment-friendly acid color fixing agent, comprising the following raw materials in parts by weight: 18 parts of isopropanol, 0.26 parts of sodium persulfate, 5.8 parts of chitosan, 6.6 parts of thirteen polyoxyethylene ethers, and 1.8 parts of squalane , 87 parts of deionized water, 2.2 parts of strong alkali powder, 5 parts of diethylene glycol monoethyl ether acetate and 4.9 parts of dimethylamine. Chitosan adopts nano-chitosan, and strong alkali powder adopts potassium hydroxide powder.
[0024] The preparation method of described high-efficiency environment-friendly acid color fixing agent, concrete steps are as follows:
[0025] Step 1, add tridecyl isomeric polyoxyethylene ether, diethylene glycol monoethyl ether acetate and dimethylamine into part of deionized water and heat to 85 degrees Celsius under stirring, then add sodium persulfate to it and completely add Keep for 2.4 hours after completion to obtain the first mixture;
[0026...
Embodiment 2
[0030] A high-efficiency and environment-friendly acidic color fixing agent, comprising the following raw materials in parts by weight: 18.8 parts of isopropanol, 0.31 parts of sodium persulfate, 6.14 parts of chitosan, 7.05 parts of thirteen polyoxyethylene ethers, and 2.04 parts of squalane , 91 parts of deionized water, 2.45 parts of strong alkali powder, 5.25 parts of diethylene glycol monoethyl ether acetate and 5.36 parts of dimethylamine. The particle size of strong alkali powder is 0.15mm.
[0031] The preparation method of described high-efficiency environment-friendly acid color fixing agent, concrete steps are as follows:
[0032] Step 1, add tridecyl isomeric polyoxyethylene ether, diethylene glycol monoethyl ether acetate and dimethylamine into part of deionized water and heat to 84 degrees Celsius under stirring, then add sodium persulfate to it and completely add Keep it for 2.8 hours after completion, and irradiate with ultraviolet light with a wavelength of 3...
Embodiment 3
[0037] A high-efficiency and environment-friendly acidic color fixing agent, comprising the following raw materials in parts by weight: 19.4 parts of isopropanol, 0.36 parts of sodium persulfate, 6.75 parts of chitosan, 7.56 parts of thirteen polyoxyethylene ethers, and 2.45 parts of squalane , 96 parts of deionized water, 3 parts of strong alkali powder, 5.65 parts of diethylene glycol monoethyl ether acetate and 5.88 parts of dimethylamine. Chitosan adopts nano-chitosan, and strong alkali powder includes a mixture of sodium hydroxide and lithium hydroxide. The particle size of strong alkali powder is 0.15mm.
[0038] The preparation method of described high-efficiency environment-friendly acid color fixing agent, concrete steps are as follows:
[0039] Step 1, add tridecyl isomeric polyoxyethylene ether, diethylene glycol monoethyl ether acetate and dimethylamine into part of deionized water and heat to 85 degrees Celsius under stirring, then add sodium persulfate to it and...
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