Direction control method of surface oxygen functional groups on coal-based hard carbon for sodium-storing cathodes
A surface oxygen and functional group technology, applied in the field of directional regulation of oxygen functional groups on the surface of coal-based hard carbon, can solve the problems of low oxygen functional group loading efficiency and waste liquid pollution, and achieve high capacity, improve porosity, and efficient loading.
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specific Embodiment approach 1
[0036] Specific implementation mode 1: This implementation mode is used for the coal-based hard carbon surface oxygen functional group directional control method for sodium storage negative electrode according to the following steps:
[0037] 1. Raw material refinement
[0038] Crushing, grinding and sieving coal raw materials in sequence to obtain fine coal powder;
[0039] 2. High temperature carbonization
[0040] Put the pulverized coal in an atmosphere furnace, carry out carbonization treatment in an inert atmosphere, and then naturally cool down to room temperature to obtain high-temperature carbonized coke;
[0041] 3. Ball milling treatment
[0042] placing the high-temperature carbonized coke in step 2 in a ball milling tank for ball milling to obtain a ball milling product; during the ball milling, the atmosphere in the ball milling tank is air atmosphere, nitrogen atmosphere or carbon dioxide atmosphere;
[0043] Four, cleaning and drying
[0044] The ball-mille...
specific Embodiment approach 2
[0049] Embodiment 2: This embodiment is different from Embodiment 1 in that: the particle size of the pulverized coal in step 1 is 20-100 mesh. Other steps and parameters are the same as those in the first embodiment.
specific Embodiment approach 3
[0050] Embodiment 3: The difference between this embodiment and Embodiment 1 or 2 is that the coal raw material in step 1 is a mixture of one or more of lignite, bituminous coal, sub-bituminous coal or anthracite in any proportion. Other steps and parameters are the same as those in Embodiment 1 or 2.
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