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Sticking glue for diamond wire silicon slice and preparation method

A technology for silicon slices and diamond wire, which is applied in the field of silicon slice sticky glue and preparation of diamond wire, can solve the problems of increasing the conductivity of cooling water or water used for degumming, easily damaging the cooling water circulation system, affecting production efficiency, etc. Degumming performance in boiled water, reducing the risk of chipping, and the effect of good water resistance and cutting fluid resistance

Inactive Publication Date: 2019-06-14
广西珀源新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In the prior art, the sticky glue of the previous generation, see the published patent CN109321185A, although it can solve the problem of degumming without adding acid and boiling, and the degumming temperature is also low, which can guarantee certain silicon chip cutting requirements, but, in use At the same time, new problems were discovered. The degumming water and cooling water used by the existing silicon wafer cutting manufacturers are in the same water circulation system, and the water will be recycled. , the degumming factor in the sticky glue will partially dissolve into the cooling water or the water used for degumming, which will greatly increase the conductivity of the cooling water or the water used for degumming, which will easily damage the cooling water circulation system or even cause a shutdown failure, which greatly affects the Production efficiency even has potential safety hazards, so a stick glue is needed, which can achieve the effect of boiling degumming without adding acid without adding degumming factor, and maintain or lower than the existing boiling degumming temperature to prevent silicon wafers from being degummed. Fragmentation or oxidation due to excessive temperature difference during degumming or cooling, affecting product yield

Method used

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  • Sticking glue for diamond wire silicon slice and preparation method
  • Sticking glue for diamond wire silicon slice and preparation method
  • Sticking glue for diamond wire silicon slice and preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A kind of diamond wire silicon slice sticky stick glue, it comprises the following raw materials in parts by weight:

[0025] Component A: 5 parts of glycidyl ester epoxy resin, 35 parts of general-purpose bisphenol A epoxy resin, 1 part of glycidyl ether, 20 parts of filler, 0.01 part of defoamer, 0.05 part of anti-settling agent and 0.01 part of coupling agent share;

[0026] Component B: 20 ​​parts of modified polythiol, 1 part of self-made m-xylylenediamine prepolymer, 1 part of accelerator, 20 parts of filler, 0.01 part of defoamer and 0.05 part of anti-settling agent;

[0027] Wherein, the self-made m-xylylenediamine prepolymer is the product described in the patent No. CN103665327B;

[0028] The glycidyl ester type epoxy resin is glycidyl ester S-182, the general-purpose bisphenol A epoxy resin is E55, and the glycidyl ether is lauryl glycidyl ether; the modified polythiol is polythiol 3800;

[0029] The coupling agent is KH-550, the accelerator is DMP-30, the ...

Embodiment 2

[0033] Component A: 10 parts of glycidyl ester epoxy resin, 75 parts of general-purpose bisphenol A epoxy resin, 5 parts of glycidyl ether, 60 parts of filler, 3 parts of defoamer, 5 parts of anti-settling agent and 3 parts of coupling agent share;

[0034] Component B: 50 parts of modified polythiol, 5 parts of self-made m-xylylenediamine prepolymer, 10 parts of accelerator, 40 parts of filler, 3 parts of defoamer and 5 parts of anti-settling agent.

[0035] Wherein, the self-made m-xylylenediamine prepolymer is the product described in the patent No. CN103665327B;

[0036] The glycidyl ester type epoxy resin is obtained by mixing glycidyl ester S-182 and glycidyl tertiary carbonic acid ester according to the ratio of 1:2 by mass ratio, and the general-purpose bisphenol A epoxy resin is E-51 and E55 according to the mass ratio of 1 : 1 mixed to obtain; Glycidyl ether is lauryl glycidyl ether; Modified polythiol is polythiol JH-3381;

[0037] The coupling agent is KH-570, th...

Embodiment 3

[0040] Component A: 8 parts of glycidyl ester epoxy resin, 55 parts of general-purpose bisphenol A epoxy resin, 3 parts of glycidyl ether, 48 parts of filler, 1.2 parts of defoamer, 2 parts of anti-settling agent and 1.8 parts of coupling agent share;

[0041] Component B: 30 parts of modified polythiol, 4 parts of self-made m-xylylenediamine prepolymer, 6 parts of accelerator, 34 parts of filler, 1.2 parts of defoamer and 2 parts of anti-settling agent.

[0042] Wherein, the self-made m-xylylenediamine prepolymer is the product described in the patent No. CN103665327B;

[0043] Described glycidyl ester type epoxy resin is glycidyl methacrylate, bisphenol A type epoxy resin is E-55; Glycidyl ether is 1,4 butanediol diglycidyl ether; Modified polythiol is Polymercaptan GMP-830 and GMP-888 are mixed according to the mass ratio of 1:1;

[0044] The coupling agent is KH-560, the accelerator is DMP-30, the defoamer is BYK-072, the anti-sedimentation agent is hydrogenated castor o...

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Abstract

The invention discloses a sticking glue for a diamond wire silicon slice and a preparation method. The sticking glue comprises a component A and a component B; the component A includes glycidyl estertype epoxy resin, general bisphenol A epoxy resin, glycidyl ether, filler, defoaming agent, anti-settling agent and coupling reagent; the component B includes modified polythiol, self-prepared m-xylylenediamine prepolymer, accelerant, filler, defoaming agent and anti-settling agent. On the basis of the prior art, the invention modifies the last generation sticking glue and provides the sticking glue for the diamond wire silicon slice and the preparation method thereof. Boiling degumming without acid can be completed without adding degumming factors; the boiling degumming temperature is 10 DEGC lower than the present one; electrical conductivity of solution in cooling water or degumming water is reduced; normal working of cooling water circulation system is guaranteed; the service life ofmachine is prolonged; production efficiency of factory is guaranteed and potential safety hazard of easiness in causing machine failure is solved.

Description

technical field [0001] The invention relates to the field of silicon chip cutting materials. More specifically, the present invention relates to a diamond wire silicon slice sticky glue and a preparation method thereof. Background technique [0002] In the prior art, the sticky glue of the previous generation, see the published patent CN109321185A, although it can solve the problem of degumming without adding acid and boiling, and the degumming temperature is also low, which can guarantee certain silicon chip cutting requirements, but, in use At the same time, new problems were discovered. The degumming water and cooling water used by the existing silicon wafer cutting manufacturers are in the same water circulation system, and the water will be recycled. , the degumming factor in the sticky glue will partially dissolve into the cooling water or the water used for degumming, which will greatly increase the conductivity of the cooling water or the water used for degumming, w...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J163/00C09J11/06C09J11/04C08G59/66C08G59/56
Inventor 吴世炆黄世文周荣晶苏光临陈韬
Owner 广西珀源新材料有限公司
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