Additive for low surface energy water-resistant and antifouling architectural coatings and preparation method thereof
An architectural coating, low surface energy technology, used in antifouling/underwater coatings, coatings, biocide-containing paints, etc., to achieve improved water resistance and antifouling properties, improved water resistance and mechanical properties, good dispersibility Effect
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Embodiment 1
[0030] (1) Put the crushed inorganic particles into the air-flow ultrafine pulverizer, spray into the surfactant and grind repeatedly, so that the edges and corners of the inorganic particles are gradually passivated under the action of rotating collision grinding, and the materials are discharged to obtain an average particle size of 7μm surface-activated high-sphericity inorganic particles; the inorganic particles are silica; the surfactant is octylphenol polyoxyethylene ether; the speed of the crushing disc repeatedly polished by the airflow ultrafine pulverizer is 5600rpm, and the speed of the impeller is 2300rpm. The air volume is 2600m 3 / h, the time is 54min; in the preparation of surface-activated high-sphericity inorganic particles, the mass ratio of inorganic particles and surfactants is 100:2.5;
[0031] (2) Grind the surface-activated high-sphericity inorganic particles and hexamethylene diisocyanate in a grinder for 52 minutes at a speed of 180rpm, then move them ...
Embodiment 2
[0037] (1) Put the crushed inorganic particles into the air-flow ultrafine pulverizer, spray into the surfactant and grind repeatedly, so that the edges and corners of the inorganic particles are gradually passivated under the action of rotating collision grinding, and the materials are discharged to obtain an average particle size of 5μm surface-activated high-sphericity inorganic particles; the inorganic particles are zinc oxide; the surfactant is nonylphenol polyoxyethylene ether; the speed of the crushing disc repeatedly polished by the airflow ultrafine pulverizer is 5000rpm, the speed of the impeller is 2000rpm, and the air volume 3000m 3 / h, the time is 60min; in the preparation of surface-activated high-sphericity inorganic particles, the mass ratio of inorganic particles to surfactants is 100:1;
[0038] (2) Grind the surface-activated high-sphericity inorganic particles and hexamethylene diisocyanate in a grinder for 60 minutes at a speed of 150 rpm, then move them i...
Embodiment 3
[0042] (1) Put the crushed inorganic particles into the air-flow ultrafine pulverizer, spray into the surfactant and grind repeatedly, so that the edges and corners of the inorganic particles are gradually passivated under the action of rotating collision grinding, and the materials are discharged to obtain an average particle size of 8 μm surface-activated high-sphericity inorganic particles; the inorganic particles are silicon dioxide; the surfactant is alkylphenol polyoxyethylene ether; the speed of the crushing disc repeatedly polished by the airflow ultrafine pulverizer is 6000rpm, and the speed of the impeller is 2500rpm. Air volume is 3000m 3 / h, the time is 50min; in the preparation of surface-activated high-sphericity inorganic particles, the mass ratio of inorganic particles to surfactant is 100:3;
[0043] (2) Grind the surface-activated high-sphericity inorganic particles and hexamethylene diisocyanate in a grinder for 40 minutes at a speed of 250rpm, then move the...
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