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Method and device for ultrasonically treating dirty oil through sulfur-containing sewage

A sewage treatment, ultrasonic technology, applied in water/sludge/sewage treatment, mechanical oscillation water/sewage treatment, hydrocarbon oil treatment, etc., can solve the problems of high water content in sewage oil, difficult treatment of extracted water, complicated process, etc. question

Pending Publication Date: 2019-08-09
QINGDAO BESTSONIC TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The purpose of the present invention is to overcome the defects of the existing ultrasonic technology, such as the addition of chemical agents, complex process, high treatment cost, high water content of the treated sewage oil, and difficulty in the treatment of extracted water, etc., to provide an ultrasonic treatment of sulfur-containing sewage. The method of dirty oil, on the one hand, avoids the corrosion of production equipment caused by the use of strong acid and strong alkali in the prior art, reduces the cost of dirty oil treatment increased by adding chemical demulsifiers and flocculants, and reduces the difficulty of processing the sewage. ; On the other hand, it simplifies the complex process of repeatedly treating dirty oil in the process of ultra-high-power ultrasonic treatment of dirty oil, and the treated dirty oil meets the index requirements of water content <5% in the mixing process of dirty oil

Method used

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  • Method and device for ultrasonically treating dirty oil through sulfur-containing sewage
  • Method and device for ultrasonically treating dirty oil through sulfur-containing sewage

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0074] Ultrasonic sulfur-containing sewage treatment device for dirty oil, including switch valve 3, delivery pump 4, pressure measurement and control 5, flow measurement and control 6, ultrasonic transducer 10, explosion-proof cabinet 11, control unit 12, sewage oil pipeline 1, and sewage oil pipeline 1 After merging with the sulfur-containing sewage pipeline 2, it is connected to the mixer 7, the mixer 7 is connected to the mixing valve 8 through the pipeline, the mixing valve 8 is connected to the ultrasonic action area 9 through the pipeline, and the ultrasonic action area 9 is connected to the mixing switch valve 13 through the pipeline connected, the mixing switch valve 13 is connected with the settling tank 14 through a pipeline.

[0075] On the pipelines connecting the dirty oil pipeline 1, the sulfur-containing sewage pipeline 2 and the mixer 7, an on-off valve 3, a delivery pump 4, a pressure measurement and control 5 and a flow measurement and control 6 are arranged ...

Embodiment 2

[0094] A method for treating dirty oil with ultrasonic sulfur-containing sewage, specifically injecting sulfur-containing sewage into the dirty oil for mixed demulsification, then strengthening the demulsification with ultrasonic waves, and finally settling in a settling tank to realize the three-phase separation of oil, water and slag, and the treated dirty oil The moisture content of the dirty oil is <5%, and the mechanical impurity content of the dirty oil is <1%.

[0095] According to the technical solution of the present invention, the sulfur-containing sewage is wastewater containing dissolved hydrogen sulfide and dissolved ammonia nitrogen produced in the petrochemical production process.

[0096] In this embodiment, material properties and process parameters:

[0097] Sulfur-containing sewage is wastewater containing dissolved hydrogen sulfide and dissolved ammonia nitrogen produced in the petrochemical production process. The sulfide (S 2- ) content 2530.3mg / L, ammon...

Embodiment 3

[0135]A method for treating dirty oil with ultrasonic sulfur-containing sewage, specifically injecting sulfur-containing sewage into the dirty oil for mixed demulsification, then strengthening the demulsification with ultrasonic waves, and finally settling in a settling tank to realize the three-phase separation of oil, water and slag, and the treated dirty oil The moisture content of the dirty oil is <5%, and the mechanical impurity content of the dirty oil is <1%.

[0136] Material properties and process parameters:

[0137] Sulfur-containing sewage is wastewater containing dissolved hydrogen sulfide and dissolved ammonia nitrogen produced in the petrochemical production process. The sulfide (S 2- ) content 12170.8mg / L, ammonia nitrogen (NH 3 -N) content 8341.6mg / L.

[0138] The mass ratio of sulfur-containing sewage to sewage oil is 2 / 10.

[0139] Preheat to 80-95°C before mixing dirty oil with sulfur-containing sewage.

[0140] The mixing strength of the mixing valve f...

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Abstract

The invention belongs to the technical field of dirty oil treatment, and particularly relates to a method and device for ultrasonically treating dirty oil through sulfur-containing sewage. The sulfur-containing sewage is injected into the dirty oil for mixed demulsification, then demulsification is ultrasonically strengthened, finally, the oil-water-slag three-phase separation is achieved throughthe sedimentation of a sedimentation tank, and the treated dirty oil has the moisture content smaller than 5% and the mechanical impurity content smaller than 1%. By means of the method, the dirty oilis demulsified by the sulfur-containing sewage, the demulsification effect is ultrasonically strengthened, the use of chemical reagents is avoided, the cost is reduced, the ideal oil-water-slag three-phase separation effect is achieved, the moisture content of the dirty oil is smaller than 5%, and the mechanical impurity content is smaller than 1%. The device for ultrasonically treating the dirtyoil through the sulfur-containing sewage can be manufactured into a skid-mounted device for vehicle-mounted movement and can also be mounted and used on an industrial site. The method and device forultrasonically treating the dirty oil through the sulfur-containing sewage are suitable for demulsification of high-moisture-content oil-water emulsions and especially suitable for dirty oil treatmentin oil fields or oil refineries.

Description

technical field [0001] The invention belongs to the technical field of waste oil treatment, and in particular relates to a method and a device for treating waste oil with ultrasonic sulfur-containing sewage. Background technique [0002] Slop oil is a type of high water content emulsified crude oil produced in the production process of oil fields or refineries. Some dirty oil is called heavy dirty oil. Heavy dirty oil has high content of mechanical impurities, high metal content, high content of solid suspended particles, high water content, high content of surfactant, etc. Heavy dirty oil mainly comes from crude oil tanks Sludge oil from processes such as undercut water, crude oil electric desalination water cut, equipment maintenance and line sweeping, sewage treatment grease trap recovery, etc.; Effective processing and utilization, after a long period of hydrothermal biochemical action, the treatment becomes more and more difficult, so it is called aging oil; the source...

Claims

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Application Information

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IPC IPC(8): C02F1/36C10G17/09C10G31/00C02F101/10C02F101/16
CPCC02F1/36C10G17/09C10G31/00C02F2101/101C02F2101/16C10G2300/205
Inventor 苟泽浩张茂锋季德伟王涛贾中辉毛金柱齐杰张达峰侯永兴邱立忠
Owner QINGDAO BESTSONIC TECH CO LTD
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