New application of dihydrochalcone compound renifolin F
A technology of dihydrochalcones and compounds, applied in the field of medical technology and health care products, to achieve the effect of inhibiting the production of inflammatory factors and improving pathological changes
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Embodiment 1
[0054] Embodiment 1: the preparation of Renifolin F
[0055] Dried copper money ephedra root (5 kg), crushed and extracted with 10L of 70% ethanol under reflux for 3 times, each time for 2 hours, the extract was concentrated under reduced pressure until it had no alcohol smell, and ethanol extract (1.8 kg) was obtained. After dispersing the extract with 1L of water, extract and degrease once with 1L of petroleum ether, then extract with ethyl acetate three times, 2L each time, combine the ethyl acetate extracts, recover under reduced pressure to obtain ethyl acetate extract (0.9 kg) .
[0056] Ethyl acetate extract was eluted by silica gel column chromatography (chloroform-methanol system) gradient (100:5-100:100), the obtained fractions were detected by thin-layer chromatography, and the fractions containing Renifolin F were combined (20 g) , after MCI column chromatography, methanol-water (0:100-100:0) gradient elution, each fraction was identified by thin-layer chromatogra...
Embodiment 2
[0060] Embodiment 2: The therapeutic effect of Renifolin F on mouse asthma
[0061] 1. Reagents: OVA (batch number: 9006-59-1) and dexamethasone (batch number: BCBV3214) were purchased from Sigma Company; Eotaxin ELISA detection kit (batch number: 2130802231), IL-4 ELISA detection kit (batch number: A20480141 ), IL-5 ELISA kit (lot number: A20580821), IL-13 ELISA kit (lot number: A21381132), IL-25 ELISA kit (lot number: M181225-007a), IL-33 ELISA kit (Lot No.: A23380314), INF-γ ELISA Kit (Lot No.: A201B81053), MUC5AC ELISA Kit (Lot No.: ZKVBMELGV3), TSLP ELISA Kit (Lot No.: A26580933), IL-2 ELISA Kit (Lot No. : A20280153), IL-6 ELISA kit (lot number: A20681154), IL-7 ELISA kit (lot number: A20781123), IL-9 ELISA kit (lot number: A20980513), IL-10 ELISA kit (Lot No.: A21090121), IL-17A ELISA Detection Kit (Lot No.: A21780741), MCP-1 ELISA Detection Kit (Lot No.: A28780431), Total IgE ELISA Detection Kit (Lot No.: A27581115) were purchased from Hangzhou Lianke Biotechnology Co...
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