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Aluminum-based composite material added with tungsten disulfide self-lubricating nanoparticles and preparation method thereof

An aluminum-based composite material and tungsten disulfide technology, which is applied in metal processing equipment, transportation and packaging, etc., can solve the problems of low wear resistance and limited application prospects, so as to improve dispersion, reduce the number of holes, and improve high-temperature hardness and the effect of high temperature wear resistance

Active Publication Date: 2020-11-03
TONGJI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the low wear resistance of aluminum alloy materials limits its application prospects in the fields of important components in automobiles and aerospace

Method used

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  • Aluminum-based composite material added with tungsten disulfide self-lubricating nanoparticles and preparation method thereof
  • Aluminum-based composite material added with tungsten disulfide self-lubricating nanoparticles and preparation method thereof
  • Aluminum-based composite material added with tungsten disulfide self-lubricating nanoparticles and preparation method thereof

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preparation example Construction

[0040] like figure 1 As shown, the preparation method of the aluminum-based composite material adding tungsten disulfide self-lubricating nanoparticles of the present invention comprises the following steps:

[0041] (1) Tungsten disulfide (WS 2 ) powder, copper powder and solid solvent are put into the high-energy ball mill and mixed evenly and cooled to obtain a composite powder;

[0042] (2) Putting the composite powder into a vacuum hot-press furnace for sintering and densification to obtain a composite ingot;

[0043] (3) In a vacuum melting furnace, melt the matrix and cast aluminum alloy, after the matrix alloy is melted, add the composite billet at 700-800°C, and stir it stably for 10-30min to obtain the mixture;

[0044] (4) Lower the furnace temperature to 550-620°C for semi-solid stirring, and stir steadily for 20-25min to obtain tungsten disulfide (WS) 2 ) a refined metal solution of nanoparticles;

[0045] (5) Preheat the casting mold to 250±10°C, add tungsten...

Embodiment 1

[0057] The preparation method of the aluminum-based composite material adding tungsten disulfide self-lubricating nanoparticles in this embodiment includes the following steps:

[0058] (1) Tungsten disulfide (WS 2 ) powder (the particle size is 40nm, accounting for 20% of the mass of the composite powder), pure copper powder (the particle size is 20 μm, accounting for 30% of the mass of the composite powder) and pure aluminum powder (the particle size is 20 μm) Uniformly mix in the high-energy ball mill, vacuum protection, the ball-to-material ratio is 15:1, the speed is 500rpm, after ball milling for 4 hours, cool to room temperature to obtain composite powder;

[0059] (2) Put the composite powder into a copper mold in a vacuum hot-press furnace for sintering and densification, with a vacuum degree of 10 - 2 Pa, the temperature is 550°C, vacuum hot pressing and sintering under the condition of 200MPa for 3h to obtain the composite ingot;

[0060] (3) In a vacuum melting ...

Embodiment 2

[0067] The preparation method of the aluminum-based composite material adding tungsten disulfide self-lubricating nanoparticles in this embodiment includes the following steps:

[0068] (1) Tungsten disulfide (WS 2 ) powder (the particle size is 40nm, accounting for 30% of the mass of the composite powder), pure copper powder (the particle size is 20 μm, accounting for 10% of the mass of the composite powder) and pure aluminum powder (the particle size is 20 μm) Mix evenly in the high-energy ball mill, vacuum protection, the ball-to-material ratio is 15:1, the rotation speed is 600rpm, and the ball mill is cooled to room temperature after 6 hours to obtain a composite powder;

[0069] (2) Put the composite powder into a copper mold in a vacuum hot-press furnace for sintering and densification, with a vacuum degree of 10 - 2 Pa, the temperature is 600°C, vacuum hot pressing and sintering under the condition of 150MPa for 3h to obtain the composite ingot;

[0070] (3) In a va...

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Abstract

The invention provides an aluminum-based composite material added with tungsten disulfide self-lubricating nanoparticles and a preparation method thereof. The preparation method is as follows: mixing and cooling tungsten disulfide powder, copper powder and aluminum powder to obtain a composite powder; The composite powder is sintered to obtain a composite ingot; after the cast aluminum alloy is melted, the composite ingot is added to the aluminum alloy melt and stirred to obtain a mixture; after the mixture is cooled to a semi-solid state, it is continuously stirred to obtain a refined metal solution; Preheating the casting mold, casting the heated refined metal solution into tungsten disulfide nano-particle reinforced aluminum-based composite material billet; the composite material billet can be heat-treated; the present invention adds disulfide disulfide to the existing cast aluminum alloy The addition of tungsten self-lubricating nanoparticles, copper powder, and copper elements can generate high-temperature-resistant precipitates in the matrix of the composite material; adding tungsten disulfide self-lubricating nanoparticles can significantly reduce the friction coefficient of the aluminum alloy material, thereby improving the composite material. High temperature wear resistance.

Description

technical field [0001] The invention belongs to the technical field of aluminum alloy composite materials, and in particular relates to an aluminum-based composite material added with tungsten disulfide self-lubricating nanoparticles and a preparation method thereof. Background technique [0002] Aluminum alloy materials have been widely used in industry due to their excellent properties such as light weight and corrosion resistance. However, the low wear resistance of aluminum alloy materials limits its application prospects in the fields of important components in automobiles and aerospace. In fact, the inherent characteristics of aluminum determine the low wear resistance of aluminum alloys. Aluminum has a low modulus of elasticity and is a soft metal with a high coefficient of friction. Therefore, it is necessary to improve the composition and reinforcement phase of the aluminum matrix to produce an aluminum matrix composite material with high temperature wear resistan...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C21/00C22C1/02C22C1/10B22F1/00B22F9/04B22F3/14C22F1/04
CPCC22C21/00C22C1/1036C22C1/1015B22F9/04B22F3/14C22F1/04B22F2009/043B22F2999/00B22F1/052C22C1/1047B22F2201/20
Inventor 翁真真葛彬乐沛雯何国求刘晓山
Owner TONGJI UNIV