Hollow fiber sleeve for protecting medical endoscope from holmium laser damage and application of sleeve
A holmium laser and endoscope technology, applied in the field of medical endoscopes, can solve problems such as damage and major maintenance costs, and achieve the effects of reducing impact, improving long-term service life, and improving impact resistance.
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Embodiment 1
[0039] In this embodiment, a method for preparing an impact-resistant and heat-insulating hollow fiber sleeve that can protect against holmium laser damage, the specific steps are as follows:
[0040] Hydrotalcite modification: take 100g of hydrotalcite FM308, and ultrasonically disperse it in 1000mL deionized water, and the ultrasonic time is 20min. Afterwards, 1000 mL of ethylene glycol was added to adjust the pH value of the mixed solution to 8, and heated and stirred at 60° C. for 30 min. Afterwards, the mixed solution containing hydrotalcite FM308 was suction-filtered, washed with deionized water, repeated three times, and dried at 60° C. for 8 hours to obtain pretreated modified hydrotalcite FM308.
[0041] SiO 2 Preparation of hollow microspheres: ultrasonically disperse 40g tetraethyl orthosilicate in 200mL ethanol solution containing 20g urea, stir at room temperature for 20min to obtain a silicon dispersion; then drop the silicon dispersion at a rate of 2 drops / seco...
Embodiment 2
[0044] In this embodiment, a method for preparing an impact-resistant and heat-insulating hollow fiber sleeve that can protect against holmium laser damage, the specific steps are as follows:
[0045] Hydrotalcite modification: take 100g of hydrotalcite FM300, and ultrasonically disperse it in 1000mL deionized water for 40min. Afterwards, 500 mL of glycerol was added to adjust the pH value of the mixed solution to 9, and heated and stirred at 60° C. for 50 min. Afterwards, the mixed solution containing hydrotalcite was suction-filtered, washed with deionized water, repeated three times, and dried at 60°C for 8 hours to obtain pretreated modified hydrotalcite FM300.
[0046] SiO 2 Preparation of hollow microspheres: ultrasonically disperse 60g of propyl orthosilicate in 400mL of ethanol solution containing 30g of urea, stir at room temperature for 40min to obtain a silicon dispersion; then add the silicon dispersion dropwise at a rate of 5 drops / second In a mixed solution of ...
Embodiment 3
[0049] In this embodiment, a method for preparing an impact-resistant and heat-insulating hollow fiber sleeve that can protect against holmium laser damage, the specific steps are as follows:
[0050] Hydrotalcite modification: take 100g of hydrotalcite HT-P, and ultrasonically disperse it in 1000mL deionized water for 30min. Afterwards, 250 mL of isobutanol was added to adjust the pH value of the mixed solution to 9, and heated and stirred at 60° C. for 40 min. Afterwards, the mixed solution containing hydrotalcite HT-P was suction-filtered, washed with deionized water, repeated 3 times, and dried at 60°C for 8 hours to obtain pretreated modified hydrotalcite HT-P.
[0051] SiO 2 Preparation of hollow microspheres: ultrasonically disperse 50g of butyl orthosilicate in 300mL of ethanol solution containing 25g of urea, stir at room temperature for 30min to obtain a silicon dispersion; then add the silicon dispersion dropwise at a rate of 3 drops / second In a mixed solution of ...
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