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Method for extracting anthocyanin by injection type cavitation, application and device used in method

An ejector-type and anthocyanin technology is applied in the field of ejector-type cavitation extraction of anthocyanins, which can solve the problems of reducing the antioxidant activity and dyeing ability of the extraction product, complicated post-processing procedures, waste of time and solvent, and the like, and achieves the extraction step. Reduced, less impurity content, less consumption

Active Publication Date: 2019-11-26
WUHAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These methods are low in cost and simple in process, and have been widely used; however, if the extraction time is too long, it will lead to the degradation of anthocyanins, waste time and solvent, and reduce the antioxidant activity and dyeing ability of the extracted products.
[0004] In recent years, laboratories have also used methods such as negative pressure cavitation, ultrasonic cavitation and high-pressure jets to extract anthocyanins, and the extraction efficiency has improved, but the single extraction amount is not large
In addition, there are enzymatic degradation and supercritical CO 2 The method is used for extraction, and the extraction effect is better, but because it contains impurities such as enzymes or hydrophilic groups, the post-treatment process is more complicated, and the environmental protection type is poor.

Method used

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  • Method for extracting anthocyanin by injection type cavitation, application and device used in method
  • Method for extracting anthocyanin by injection type cavitation, application and device used in method

Examples

Experimental program
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Effect test

Embodiment 1

[0031] like figure 1 and 2 As shown, a device used in a method for extracting anthocyanin by ejection cavitation; includes an ejection cavitation generator 1 and a circulating water tank 7, and the ejection cavitation generator 1 includes first inlets connected in sequence Water pipe 101, nozzle 102, suction chamber 103, throat pipe 104 and diffuser pipe 105, the outlet of the nozzle 102 extends into the suction chamber 103, the contact section between the nozzle 102 and the suction chamber 103 and the throat pipe 104 is in a shrinking structure, so The side wall of the suction chamber 103 is provided with a second water inlet pipe 106, the first water inlet pipe 101, the second water inlet pipe 106 and the diffuser pipe 105 are respectively connected to the circulating water tank 7 through pipelines, and the first water inlet pipe 101 and the circulation The water tanks 7 are communicated through the centrifugal pump 6 .

[0032] The ratio of the flow area of ​​the throat 1...

Embodiment 2

[0038] A method for extracting and injecting cavitation to extract anthocyanins in purple sweet potato, comprising:

[0039] 1. Take fresh purple sweet potato slices or cut into pieces, grind to 60 mesh after dehydration treatment, fully mix purple sweet potato powder and 0.1M citric acid aqueous solution at room temperature according to the solid-to-liquid ratio of 0.005 (mass: volume), and measure the pH of the mixture The value is between 2.0 and 2.5.

[0040] 2. Add ultra-pure water to the circulating water tank 7 of the injection-type cavitation extraction device. After starting the device, adjust the valves until the inlet pressure is 390kPa and the outlet pressure is 130kPa, then shut down the device and drain the water in the circulating water tank 7 ; Add the solid-liquid mixture sample in the circulating water tank 7, the volume of the extracted mixed solution is 50L, and the starting device starts to extract. After 25 minutes of extraction, the supernatant after ce...

Embodiment 3

[0043] 1. After dehydrating the blueberries, grind them to 60 mesh, mix the blueberry powder and 0.1M citric acid aqueous solution at room temperature at a solid-to-liquid ratio of 0.01 (mass:volume), and measure the pH value of the mixture in the range of 2.0 to 2.5 between.

[0044] 2. Add ultra-pure water to the circulating water tank 7 of the injection-type cavitation extraction device. After starting the device, adjust the valves until the inlet pressure is 300kPa and the outlet pressure is 100kPa, then shut down the device and drain the water in the circulating water tank 7 ; Add the solid-liquid mixture sample to the circulating water tank 7, the volume of the extracted mixed solution is 60L, start the device to start extraction, and the extraction time is 30min.

[0045] 3. After centrifuging the mixed solution obtained after the extraction, take the supernatant and concentrate it under reduced pressure to obtain a reddish-purple concentrated solution, which is the blu...

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Abstract

The invention relates to the technical field of extraction of effective components of plants, in particular to a method for extracting anthocyanin by injection type cavitation, application and a device used in the method. The method for extracting the anthocyanin by injection type cavitation comprises the following steps: (1) pretreating a raw material to be extracted, and then mixing the raw material to be extracted with an extraction solvent according to a certain solid-liquid ratio; (2) extracting the solid-liquid mixture in the step (1) by using an injection type cavitation extraction method; and (3) after extraction is finished, taking supernatant after the solid-liquid mixture is centrifuged, and carrying out suction filtration to obtain an anthocyanin solution. The extracting methodis high in efficiency, low in energy consumption, high in treatment capacity and simple in process, the consumption of the solvent required by extraction of the method is small, the cost is low, theimpurity content after extraction is small, and further purification is facilitated. The concentration of the anthocyanin in the anthocyanin solution extracted by the extracting method is 8.5-10 mu g / mL, and the concentration of the anthocyanin obtained by the method is higher than the concentration of the anthocyanin obtained by a traditional solvent extracting method by 25%-50%.

Description

technical field [0001] The invention relates to the technical field of extraction of plant effective components, in particular to a method, application and device for extracting anthocyanins by injection cavitation. Background technique [0002] Plant-derived anthocyanin pigments are flavonoid compounds, most of which exist in the form of stable anthocyanins, and a single angiosperm can sometimes contain as many as dozens of anthocyanins. The number and type of substituents of different ring A and ring B constitute more than 20 known aglycones, which constitute more than 300 known anthocyanins. "Anthocyanins", which are usually used as finished products in the food industry, are a general term for a variety of glycosides with similar chemical properties and molecular structures. [0003] Traditional extraction methods of anthocyanins, such as solvent extraction and pressurized solvent extraction, use solvents to extract at room temperature or under pressure to increase the ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D11/02C07H1/08C07H17/065
CPCB01D11/02C07H1/08C07H17/065
Inventor 龙新平王炯王文婷梁蕴致唐巾洁徐默涵赵凯
Owner WUHAN UNIV