Preparation method of agricultural and forestry waste adsorbing material for treatment of printing and dyeing wastewater
A technology of agricultural and forestry waste and adsorption materials, which is applied in the field of preparation of agricultural and forestry waste adsorption materials for printing and dyeing wastewater treatment, can solve the problems of destroying human health, organic mutation, and causing cancer, and achieve good flocculation and complexation adsorption. Low rate, safe and convenient to use
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Embodiment 1
[0022] Embodiment 1: as figure 1 As shown, the present invention provides a technical solution, a method for preparing an agricultural and forestry waste adsorption material for printing and dyeing wastewater treatment, comprising the following steps:
[0023] S1. Premix the short-chain acid and the long-chain acid, and pre-react at a certain temperature for a certain period of time to obtain a highly active mixed acid;
[0024] S2. Blend bagasse, straw, rice straw fiber waste and mixed acid evenly, adjust a certain moisture content, put it into a microwave device, react at a certain power for a certain period of time, and obtain a crude mixed acid cellulose ester;
[0025] S3, after washing, suction filtration and drying, a mixed acid cellulose ester product is obtained;
[0026] S4. Using sodium alginate as a forming agent, heating and blending with the prepared mixed acid cellulose ester, cooling and then crosslinking and solidifying to obtain a spherical adsorbent.
[00...
Embodiment 2
[0034] Embodiment 2: as figure 1 As shown, the present invention provides a technical solution, a method for preparing an agricultural and forestry waste adsorption material for printing and dyeing wastewater treatment, comprising the following steps:
[0035] S1. Premix the short-chain acid and the long-chain acid, and pre-react at a certain temperature for a certain period of time to obtain a highly active mixed acid;
[0036] S2. Blend bagasse, straw, rice straw fiber waste and mixed acid evenly, adjust a certain moisture content, put it into a microwave device, react at a certain power for a certain period of time, and obtain a crude mixed acid cellulose ester;
[0037] S3, after washing, suction filtration and drying, a mixed acid cellulose ester product is obtained;
[0038] S4. Using sodium alginate as a forming agent, heating and blending with the prepared mixed acid cellulose ester, cooling and then crosslinking and solidifying to obtain a spherical adsorbent.
[00...
Embodiment 3
[0046] Embodiment 3: as figure 1 As shown, the present invention provides a technical solution, a method for preparing an agricultural and forestry waste adsorption material for printing and dyeing wastewater treatment, comprising the following steps:
[0047] S1. Premix the short-chain acid and the long-chain acid, and pre-react at a certain temperature for a certain period of time to obtain a highly active mixed acid;
[0048] S2. Blend bagasse, straw, rice straw fiber waste and mixed acid evenly, adjust a certain moisture content, put it into a microwave device, react at a certain power for a certain period of time, and obtain a crude mixed acid cellulose ester;
[0049] S3, after washing, suction filtration and drying, a mixed acid cellulose ester product is obtained;
[0050] S4. Using sodium alginate as a forming agent, heating and blending with the prepared mixed acid cellulose ester, cooling and then crosslinking and solidifying to obtain a spherical adsorbent.
[00...
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