Hybrid porous monolithic material, and preparation method and application thereof
A monolithic material and hybridization technology, applied in chemical instruments and methods, and other chemical processes, can solve problems such as poor stability, easy swelling, and poor mechanical strength of organic monolithic columns
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[0024] Preparation of POSS-SH functional monomer: First, take 15mL of mercaptopropyltrimethoxysilane (MPTS) and dissolve it in 360mL of methanol, add 30mL of concentrated hydrochloric acid (36% to 38%) dropwise to the solution, and in an oil bath at 90°C Reflux reaction for 24 hours; after the reaction is completed, cool the reaction solution in an ice bath (-4°C-4°C) to obtain a crude product, wash the crude product with methanol three times to remove residual mercaptopropyltrimethoxysilane; then, use di Dissolve the obtained crude product in methyl chloride, add water to the solution for extraction, collect the dichloromethane layer, then add water for extraction, repeat three times, finally collect dichloromethane, add anhydrous sodium sulfate to it and dry overnight; finally, the obtained The solution was distilled under reduced pressure to obtain the product POSS-SH. The obtained POSS-SH was dissolved in tetrahydrofuran solution (50.0%, w / v, mg / ml) for use.
[0025] The ...
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