A kind of equipment and process for fully automatic continuous production of antioxidant rd
An anti-aging agent, fully automatic technology, applied in the direction of organic chemistry, etc., can solve the problems of unstable product quality, low equipment utilization, low production efficiency, etc., to achieve the effect of improving equipment utilization, reducing post personnel, and improving stability
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0047] like figure 1 As shown, a fully automatic and continuous production of anti-aging agent RD equipment includes a salt forming tank 5, a polycondensation tank 6, a buffer tank 9, a neutralization tank 10 and a stratifier 13. Salt forming tank 5, polycondensation tank 6, buffer tank 9, neutralization tank 10 and stratifier 13 are connected in series through pipelines.
[0048] There is a steam coil 16 in the salt forming kettle 5, and the temperature is controlled in chain. The salt-forming kettle 5 also has a stirring device, and there are two layers of paddles up and down, the upper paddle is a downward pressure type, and the lower paddle is an upturned type to prevent the formation of a vortex.
[0049] The salt forming kettle 5 is connected to the hydrochloric acid pump 2 and the aniline pump 1 through two pipelines respectively. The inlet of the aniline pump 1 is connected to the aniline or recovery aniline storage tank, the outlet of the aniline pump 1 is connected...
Embodiment 2
[0067] Adopt the method for the full-automatic continuous production of anti-aging agent RD of the equipment of embodiment 1, comprise steps:
[0068] 1) Pump aniline or recovered aniline and hydrochloric acid into the salt-forming kettle 5, and the feeding amount is controlled by the aniline feed amount regulating valve group 3 and the hydrochloric acid feeding amount regulating valve group 4; the salt-forming material reaches the overflow of the salt-forming kettle 5 Automatically overflow to polycondensation kettle 6 when opening;
[0069] Among them, the feed rate of aniline was controlled at 9 L / h, and the feed rate of hydrochloric acid (30% by mass) was controlled at 4 L / h; the residence time of the salt-forming material in the salt-forming tank was 2.5 h; the salt-forming temperature was 120°C;
[0070] 2) Acetone or recovered acetone is pumped into the polycondensation kettle 6, and the feed amount is adjusted according to the set material ratio through the acetone fee...
PUM
| Property | Measurement | Unit |
|---|---|---|
| softening point | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More