Treatment solution for film formation
A technology for treating liquid and chemical formation treatment, which is applied in the direction of pretreatment surface, device for coating liquid on the surface, coating, etc., which can solve the problem of inability to meet corrosion resistance and achieve the effect of improving corrosion resistance.
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Embodiment 1
[0111] Prepared acrylic silicone resin (weight-average molecular weight: about 20,000, alkoxysilyl content: 40% by mass) 10% by mass, bisphenol A type epoxy resin 10% by mass, and propylene glycol monoethyl ether 80% by mass % of the mixture. Next, 3 parts by mass of water and 2 parts by mass of aluminum monoacetylacetonate diethylacetoacetate were added to 100 parts by mass of the mixed liquid to prepare a treatment liquid for film formation.
[0112] On the other hand, phosphorylation treatment was performed by immersing a metal material (magnesium alloy AZ91 substrate (size: 100×60×0.3 mm)) in 50 g / L of a sodium phosphate aqueous solution adjusted to 60° C. for 3 minutes.
[0113] The obtained metal material having a phosphating-treated coating was sprayed with the above-prepared coating-forming treatment solution, and heat-treated at 200° C. for 30 minutes using a drier to form a coating.
Embodiment 2
[0115] It carried out similarly to Example 1 except having performed the zirconium conversion process instead of the phosphorylation process on the metal material. The zirconium conversion treatment was carried out by immersing the metal material in 100 g / L of an aqueous ammonium zirconium nitrate solution whose temperature was adjusted to 60° C. for 1 minute.
Embodiment 3
[0117] It carried out similarly to Example 1 except having performed trivalent chromium conversion process instead of phosphoric acid conversion process with respect to a metal material. The trivalent chromium conversion treatment was carried out by immersing the metal material in 100 g / L of a trivalent chromium nitrate aqueous solution whose temperature was adjusted to 40° C. for 1 minute.
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