Mangnolia officinalis burst bead essential oil and preparation method thereof

A technology of popping essential oils and magnolia bark, which is applied in the direction of essential oils/fragrances, fat production, etc., which can solve the problems of affecting the formation of popping beads, thin flavor and fragrance, and limited optional fragrance types, so as to reduce irritation, rich aroma, and high quality. stable effect

Active Publication Date: 2020-02-07
HUBEI CHINA TOBACCO IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The essence used for the popcorn essential oil is basically a synthetic flavor, which plays an important role in improving the aroma of the popcorn essential oil and enriching the aroma of the smoke. , wall materials, etc., resulting in an unstable state during the online molding process of popping beads, which affects the molding of popping beads, and natural flavors are restricted by the tobacco additive license list, and the optional flavors are limited
[0003]The trunk bark, root bark and branch bark of Magnoliaceae Magnolia officinalis is a commonly used traditional Chinese medicine. The effect of reducing dampness and harmonizing the stomach, pharmacology has proved that it has a significant effect of lowering blood pressure and inhibiting pathogenic microorganisms. Magnolol and Magnolol, Eugenol-4'-O-β-D-Glucopyranoside, Magnolia A, Magnolia B, Magnolia C, Magnolia D , Magnolia lignan E, Magnolia lignan F, Magnolia lignan G, Magnolia lignan H, Magnolia lignan I, borneol magnolol and other components, all kinds of Magnolia officinalis extracts have A fresh, spicy and sweet aroma, harmonious with the smoke, and can significantly reduce the throat irritation when smoking cigarettes. It is a good natural flavor for tobacco. At present, no related extracts of magnolia bark have been used in cigarettes. Reports with Flavors and Fragrances

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Take 100g Magnolia officinalis and grind and sieve to make the particle size within 2-10mm; add 200ml 20%-40% ethanol aqueous solution, 5U cellulase, ultrasonic extraction power 10-20kHz, 30-45°C, extract 5 After -10h, centrifuge at 1000r / min for 3-5min until the water and oil are separated, and take the oil phase to obtain magnolia oleoresin;

[0028] Mix commercially available 5g green tea essential oil, 5g fig essential oil, 10g magnolia oleoresin prepared above, 0.5g commercially available vitamin K, and 0.3g fat-soluble coenzyme Q10 into 1g Tween 80, stir evenly, and dissolve in 500g three Glyceryl caprylate, continue to stir for 3-5 hours, filter to remove insoluble matter, and collect the filtrate; degas the filtrate under negative pressure at 20-60°C for 0.5-2 hours, and let it stand for 2-24 hours to obtain the Magnolia officinalis essential oil.

Embodiment 2

[0030] Take 100g Magnolia officinalis and grind and sieve to make the particle size within 2-10mm; add 200ml 20%-40% ethanol aqueous solution, 5U cellulase, ultrasonic extraction power 10-20kHz, 30-45°C, extract 5 After -10h, centrifuge at 1000r / min for 3-5min until the water and oil are separated, and take the oil phase to obtain magnolia oleoresin;

[0031] Mix 1g of commercially available green tea essential oil, 1g of fig essential oil, 5g of magnolia oleoresin prepared above, 0.1g of commercially available vitamin K, and 0.1g of fat-soluble coenzyme Q10 into 0.1g of Tween 80, stir evenly, and dissolve in 100g Glyceryl tricaprylate, continue to stir for 3-5 hours, filter to remove insoluble matter, and collect the filtrate; degas the filtrate under negative pressure at 20-60°C for 0.5-2 hours, and let it stand for 2-24 hours to obtain the Magnolia officinalis essential oil.

Embodiment 3

[0033] Take 100g Magnolia officinalis and grind and sieve to make the particle size within 2-10mm; add 200ml 20%-40% ethanol aqueous solution, 5U cellulase, ultrasonic extraction power 10-20kHz, 30-45°C, extract 5 After -10h, centrifuge at 1000r / min for 3-5min until the water and oil are separated, and take the oil phase to obtain magnolia oleoresin;

[0034] Mix 3g of commercially available green tea essential oil, 3g of fig essential oil, 8g of magnolia oleoresin prepared above, 0.3g of commercially available vitamin K, and 0.2g of fat-soluble coenzyme Q10 into 0.5g of Tween 80, stir evenly, and dissolve in 300g Glyceryl tricaprylate, continue to stir for 3-5 hours, filter to remove insoluble matter, and collect the filtrate; degas the filtrate under negative pressure at 20-60°C for 0.5-2 hours, and let it stand for 2-24 hours to obtain the Magnolia officinalis essential oil.

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PUM

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Abstract

The invention discloses mangnolia officinalis burst bead essential oil and a preparation method thereof. The mangnolia officinalis burst bead essential oil comprises 1 to 5 parts of green tea essential oil, 1 to 5 parts of fig essential oil, 5 to 10 parts of mangnolia officinalis oil resin, 0.1 to 1 part of tween 80, 100 to 500 parts of tricaprylin, 0.1 to 0.5 part of fat-soluble vitamin and 0.1 to 0.3 part of fat-soluble antioxidant. The preparation method comprises the following steps: grinding the mangnolia officinalis until the grain diameter is 2 to 10 mm; adding a solvent and cellulase,performing ultrasonic heating and extraction for 5 to 10 hours, performing centrifugation at 1000 r / min for 3 to 5 minutes until water and oil are separated and taking the oil phase to obtain the mangnolia officinalis oil resin; dissolving 1 to 5 parts of green tea essential oil, 1 to 5 parts of fig essential oil, 5 to 10 parts of mangnolia officinalis oil resin, 0.1 to 1 part of tween 80, 0.1 to0.5 part of fat-soluble vitamin and 0.1 to 0.3 part of fat-soluble coenzyme Q10 into 100 to 500 parts of tricaprylin, filtering and collecting filtrate; and degassing the filtrate at 20 to 60 DEG C and under negative pressure for 0.5 to 2 hours and standing for 2 to 24 hours to obtain the mangnolia officinalis burst bead essential oil. The burst bead essential oil has high mangnolia officinalis extract content and long preservation time, does not react with a wall material, is formed stably, and has comfortable, pure and natural fragrance, durable and stable fragrance and controllable fragrance strength.

Description

technical field [0001] The invention relates to the field of flavors and fragrances for tobacco, in particular to a Magnolia officinalis essential oil and a preparation method thereof. Background technique [0002] Popping beads is a special process for flavoring cigarette auxiliary materials and a major innovation in the tobacco industry. The method of popping beads and flavoring improves the safety of cigarette products and greatly enriches the types of flavoring materials. In recent years, major tobacco companies have increased investment in the research and development of puffed pearls, and launched a large number of puffed puffed cigarette products with their own characteristics. important direction. The essence used for the popcorn essential oil is basically a synthetic flavor, which plays an important role in improving the aroma of the popcorn essential oil and enriching the aroma of the smoke. , wall materials, etc., resulting in an unstable state during the online...

Claims

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Application Information

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IPC IPC(8): C11B9/00C11B9/02
CPCC11B9/00C11B9/0015C11B9/0061C11B9/0034C11B9/0053C11B9/022C11B9/025C11B9/027
Inventor 蹇顺华吴成刚张瑞萍齐富友刘吟邵兴伟
Owner HUBEI CHINA TOBACCO IND
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